乙酰溴-α-D-葡萄糖合成路线 （共 502 条）
反应条件
mercury(II) diacetate in benzene T=120°C; 5 h; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Uvarova, Nina I.; Atopkina, Lyubov N.; Elyakov, Georgi B.
Carbohydrate Research, 1980 , vol. 83, p. 33 - 42
反应条件
anhydrous cadmium carbonate in toluene 0.5 h; Heating; Yield given. Yields of byproduct given;
参考文献
Uvarova, Nina I.; Atopkina, Lyubov N.; Elyakov, Georgi B.
Carbohydrate Research, 1980 , vol. 83, p. 33 - 42
反应条件
diff. solvents (benzene, nitromethane, toluene, chloroform); catalysts (Hg(OAc)2, Hg(CN)2, CdCO3, Ag2O, Ag2CO3, HgO/HgBr2, HgBr2*HBr); varying react. conditions; Product distribution;
参考文献
Uvarova, Nina I.; Atopkina, Lyubov N.; Elyakov, Georgi B.
Carbohydrate Research, 1980 , vol. 83, p. 33 - 42
反应条件
silver trifluoromethanesulfonate in dichloromethane T=-10°C; 0.25 h;
参考文献
Millar, Alan; Kim, Ki Hyup; Minster, David K.; Ohgi, Tadaaki; Hecht, Sidney M.
Journal of Organic Chemistry, 1986 , vol. 51, # 2 p. 189 - 196
反应条件
lutidine; tetrabutylammomium bromide in chloroform T=45°C; 24 h;
参考文献
Millar, Alan; Kim, Ki Hyup; Minster, David K.; Ohgi, Tadaaki; Hecht, Sidney M.
Journal of Organic Chemistry, 1986 , vol. 51, # 2 p. 189 - 196
反应条件
1: 86 percent / potassium carbonate / acetone; toluene / 1 h 2: NaOMe / methanol 3: mercuric nitrate / acetonitrile View Scheme
参考文献
Adelhorst, Kim; Bjoerkling, Fredrik; Godtfredsen, Sven Erik; Kirk, Ole
Synthesis, 1990 , # 2 p. 112 - 115
反应条件
1: 70 percent / Hg(CN)2, HgBr2 / acetonitrile / 12 h 2: 90 percent / potassium tert-butoxide, H2O / methanol / 5 h View Scheme
参考文献
Helferich; Goerdeler
Chemische Berichte, 1940 , vol. 73, p. 532,539
反应条件
pyridine; silver(l) oxide
参考文献
Wagner; Hoerhammer
Zeitschrift fuer Naturforschung, 1969 , vol. 24b, p. 1408,1413
反应条件
1: 1.80 g / silver oxide; MgSO4 / diethyl ether / 24 h / 20 °C 2: pyridine / benzene / 48 h / 4 °C View Scheme
参考文献
Rubnov; Kashman; Rabinowitz; Schlesinger; Mechoulam
Journal of Natural Products, 2001 , vol. 64, # 7 p. 993 - 996
反应条件
potassium hydroxide; chloroform
参考文献
Montgomery et al.
Journal of Organic Chemistry, 1946 , vol. 11, p. 301,305
