乙酰溴-α-D-葡萄糖合成路线 （共 502 条）
反应条件
N(Et)4ClO4 in acetonitrile Arylation; ElectrolysisAg cathode; controlled potential; Further byproducts given;
参考文献
Physical Chemistry Chemical Physics, , vol. 1, # 12 p. 2989 - 2995
反应条件
Yield given. Multistep reaction;
参考文献
Carbohydrate Research, , vol. 198, # 2 p. 223 - 234
反应条件
Yield given. Multistep reaction;
参考文献
Carbohydrate Research, , vol. 198, # 2 p. 223 - 234
反应条件
Yield given. Multistep reaction;
参考文献
Carbohydrate Research, , vol. 198, # 2 p. 223 - 234
反应条件
N(Et)4ClO4 in acetonitrile Elimination; Dimerization; Acetylation; Electrochemical reaction; Product distribution; Further Variations:different charge and supporting electrolyte;
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 65, # 6 p. 881 - 898
反应条件
pyridine 1.) CH2Cl2, reflux, 8 h; other solvents, other reaction time, pyridine presence, 2.) room temperature, 24 h; other tetra-O-acetyl D-glucopyranosyl halides, other zinc salts of alcohols, phenols, thiols; Product distribution;
参考文献
Carbohydrate Research, , vol. 285, p. 159 - 165
反应条件
1: 1.) methyl α-D-glucopyranoside, LiBr / 1.) DMF, electrolysis (Pt, -2 V, 20-40 mA cm-2), 20 deg C, 7 h, 2.) DMF, 20 deg C, 14 h 2: pyridine View Scheme
参考文献
Kochetkov, Nicolay K.; Klimov, Evgeny M.; Malysheva, Nelly N.; Demchenko, Alexey V.
Carbohydrate Research, 1991 , vol. 212, p. 77 - 91
反应条件
2,4,6-trimethyl-pyridine; silver tetrafluoroborate in acetonitrile 4 h; Ambient temperature;
参考文献
Carbohydrate Research, , vol. 144, p. 137 - 147
反应条件
T=-15 - 50°C; Mechanism;
参考文献
Isbell; Frush
Journal of Research of the National Bureau of Standards (United States), 1949 , vol. 43, p. 161,165, 166
反应条件
1: acetic acid; zinc / water / -20 - 0 °C / Inert atmosphere 2: methanol; sodium methylate / 20 °C / Inert atmosphere 3: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide; mineral oil / 4 h / 0 - 60 °C / Inert atmosphere View Scheme
参考文献
Humenik, Martin; Kutschy, Peter; Kovacik, Vladimir; Bekesova, Slavka
Collection of Czechoslovak Chemical Communications, 2005 , vol. 70, # 4 p. 487 - 506
