乙酰溴-α-D-葡萄糖合成路线 (共 502 条)
反应条件
hydrogen bromide; acetic acid in dichloromethane T=20°C; 2 h;
参考文献
US8637648 B1, ;
Page/Page column 28 ;
反应条件
pyridine; (PhO)3P*Br2 in dichloromethane 0.0833333 h;
参考文献
Mani; Kanakamma
Synthetic Communications, 1992 , vol. 22, # 15 p. 2175 - 2182
反应条件
acetyl-bromide; zinc dibromide in dichloromethane T=22°C; 24 h;
参考文献
Zhang, Zhiyuan; Magnusson, Goeran
Carbohydrate Research, 1996 , vol. 295, p. 41 - 55
反应条件
hydrogen bromide in acetic acid
参考文献
WO2006/86562 A2, ;
Page/Page column 250-251; 257; 316 ;
反应条件
acetyl-bromide; zinc dibromide in dichloromethane T=22°C; Yields of byproduct given;
参考文献
Zhang, Zhiyuan; Magnusson, Goeran
Carbohydrate Research, 1996 , vol. 295, p. 41 - 55
反应条件
1: D-glucopyranose With perchloric acid; acetic anhydride T=30 - 40°C; 0.5 h; 2: acetyl-bromide With water T=20°C; 2 h;
参考文献
Datoussaid, Yazid; Othman, Adil A.; Kirsch, Gilbert
South African Journal of Chemistry, 2012 , vol. 65, p. 30 - 35
反应条件
acyl bromide; zinc dibromide in dichloromethane 12 h; Heating;
参考文献
Grynkiewicz, Grzegorz; Konopka, Miroslawa
Polish Journal of Chemistry, 1987 , vol. 61, # 1-3 p. 149 - 153
反应条件
trichloromonobromomethane in tetrachloromethane Irradiation;
参考文献
Tetrahedron Letters, , vol. 31, # 8 p. 1133 - 1136
反应条件
bromine in dichloromethane-d2 T=-45 - 20°C; 0.5 h; Title compound not separated from byproducts;
参考文献
Chemistry - A European Journal, , vol. 11, # 21 p. 6159 - 6174
反应条件
acetyl-bromide; acetic acid
参考文献
Journal of the American Chemical Society, , vol. 76, p. 3224