乙酰溴-α-D-葡萄糖合成路线 (共 502 条)
反应条件
Yield given. Multistep reaction;
参考文献
Carbohydrate Research, , vol. 198, # 2 p. 223 - 234
反应条件
N(Et)4ClO4 in acetonitrile Elimination; Dimerization; Acetylation; Electrochemical reaction; Product distribution; Further Variations:different charge and supporting electrolyte;
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 65, # 6 p. 881 - 898
反应条件
pyridine 1.) CH2Cl2, reflux, 8 h; other solvents, other reaction time, pyridine presence, 2.) room temperature, 24 h; other tetra-O-acetyl D-glucopyranosyl halides, other zinc salts of alcohols, phenols, thiols; Product distribution;
参考文献
Carbohydrate Research, , vol. 285, p. 159 - 165
反应条件
1: 43 percent / aq. NaOH / acetone / 7 h / Ambient temperature 2: 6mM methanolic MeONa / 5 h / Ambient temperature View Scheme
参考文献
Robinson
Biochemical Journal, 1956 , vol. 63, p. 39,40
反应条件
β-cyclodextrin; zinc in water T=20°C; 0.5 h; Sonication;
参考文献
Zhao, Jinzhong; Shao, Huawu; Wu, Xin; Shi, Shaojing
Chinese Journal of Chemistry, 2011 , vol. 29, # 7 p. 1434 - 1440
反应条件
Ni(COD)2; Pybox in N,N-dimethyl-formamide T=25°C; Negishi coupling reaction; 12 h; optical yield given as percent de;
参考文献
Gong, Hegui; Gagne, Michel R.
Journal of the American Chemical Society, 2008 , vol. 130, # 36 p. 12177 - 12183
反应条件
Ag(1+)*C14H24AgN4O2(1+)*2Cl(1-) in acetonitrile T=25°C; 3 h; Darkness; stereoselective reaction;
参考文献
Talisman, Ian J.; Kumar, Vineet; Deschamps, Jeffrey R.; Frisch, Mark; Malhotra, Sanjay V.
Carbohydrate Research, 2011 , vol. 346, # 15 p. 2337 - 2341
反应条件
Chromium (III) chloride; manganese; N,N,N',N,-tetramethylethylenediamine in N,N-dimethyl-formamide T=0°C; 0.75 h;
参考文献
Spencer, Roxanne P.; Schwartz, Jeffrey
Journal of Organic Chemistry, 1997 , vol. 62, # 13 p. 4204 - 4205
反应条件
Ag(1+)*C22H24AgN4(1+)*2Cl(1-) in acetonitrile T=25°C; 3 h; Darkness; stereoselective reaction;
参考文献
Talisman, Ian J.; Kumar, Vineet; Deschamps, Jeffrey R.; Frisch, Mark; Malhotra, Sanjay V.
Carbohydrate Research, 2011 , vol. 346, # 15 p. 2337 - 2341
反应条件
Ag(1+)*C22H24AgN4(1+)*2Cl(1-) in acetonitrile T=25°C; 3 h; Darkness; stereoselective reaction;
参考文献
Talisman, Ian J.; Kumar, Vineet; Deschamps, Jeffrey R.; Frisch, Mark; Malhotra, Sanjay V.
Carbohydrate Research, 2011 , vol. 346, # 15 p. 2337 - 2341