乙酰溴-α-D-葡萄糖合成路线 (共 502 条)
反应条件
1-methyl-1H-imidazole; zinc in ethyl acetate 3 h; Title compound not separated from byproducts;
参考文献
Somsak, Laszlo; Madaj, Janusz; Wisniewski, Andrzej
Journal of Carbohydrate Chemistry, 1997 , vol. 16, # 7 p. 1075 - 1087
反应条件
N(Et)4ClO4 in acetonitrile Arylation; ElectrolysisAg cathode; controlled potential; Further byproducts given;
参考文献
Rondinini, Sandra; Mussini, Patrizia R.; Cantu, Giovanni; Sello, Guido
Physical Chemistry Chemical Physics, 1999 , vol. 1, # 12 p. 2989 - 2995
反应条件
N(Et)4ClO4 in acetonitrile Elimination; Dimerization; Acetylation; Electrochemical reaction; Product distribution; Further Variations:different charge and supporting electrolyte;
参考文献
Rondinini, Sandra B.; Mussini, Patrizia R.; Crippa, Federico; Petrone, Michela; Sello, Guido
Collection of Czechoslovak Chemical Communications, 2000 , vol. 65, # 6 p. 881 - 898
反应条件
1-methyl-1H-imidazole; zinc in ethyl acetate Heatingeffect of additives on product yields; Product distribution;
参考文献
Somsak, Laszlo; Madaj, Janusz; Wisniewski, Andrzej
Journal of Carbohydrate Chemistry, 1997 , vol. 16, # 7 p. 1075 - 1087
反应条件
potassium hydroxide; N-benzyl-N,N,N-triethylammonium chloride in chloroform; water Koenigs-Knorr reaction; Heating;
参考文献
Pavlov; Sokolov; Zakharov
Russian Journal of General Chemistry, 2001 , vol. 71, # 11 p. 1811 - 1814
反应条件
pyridine; sodium hydroxide 1.) acetone, RT, 6 h, 2.) 90 deg C, 50 min; Yield given. Multistep reaction;
参考文献
Shao, Yu; Li, Yun Long; Zhou, Bing Nan
Phytochemistry, 1996 , vol. 41, # 6 p. 1593 - 1598
反应条件
carbon disulfide; Na2S*9H2O in N,N-dimethyl-formamide T=20°C; 0.0833333 h; SolventTime; stereoselective reaction;
参考文献
Jana, Manas; Misra, Anup Kumar
Journal of Organic Chemistry, 2013 , vol. 78, # 6 p. 2680 - 2686
反应条件
carbon disulfide; Na2S*9H2O in N,N-dimethyl-formamide T=20°C; 0.0833333 h; stereoselective reaction;
参考文献
Journal of Organic Chemistry, , vol. 78, # 6 p. 2680 - 2686
反应条件
1: With N,N-dimethyl-thioformamide; water T=100°C; 0.0833333 h; 2: With methanol 0.166667 h;
参考文献
Journal of Carbohydrate Chemistry, , vol. 22, # 2 p. 73 - 78
反应条件
1: 95 percent / acetone / 0.5 h / Heating 2: 96 percent / K2CO3, NaHSO3 / acetone; H2O / Ambient temperature View Scheme
参考文献
Saito, Setsuo; Tsuchiya, Tomofusa
Chemical & Pharmaceutical Bulletin, 1985 , vol. 33, # 2 p. 503 - 508