乙酰溴-α-D-葡萄糖合成路线 （共 502 条）
反应条件
1: 38 percent / Ag2CO3 / acetonitrile / 8 h / 20 °C 2: 98 percent / DMAP; pyridine / CH2Cl2 / 0.5 h 3: 40 percent / Pd(OAc)2; benzyltriethylammonium chloride; Bu3N / acetonitrile / 1.5 h / 85 °C 4: 94 percent / NaOMe / methanol / 1 h / 20 °C View Scheme
参考文献
Orsini, Fulvia; Pelizzoni, Francesca; Bellini, Barbara; Miglierini, Giuliana
Carbohydrate Research, 1997 , vol. 301, # 3-4 p. 95 - 109
反应条件
sodium hydroxide in acetone 7 h; Ambient temperature;
参考文献
Malet, Carles; Viladot, Josep Lluis; Ochoa, Ana; Gallego, Belen; Brosa, Carme; Planas, Antoni
Carbohydrate Research, 1995 , vol. 274, p. 285 - 302
反应条件
1: mercury(II) cyanide / nitromethane 2: 19.2 g / sodium methoxide / methanol 3: 75 percent / p-toluenesulfonic acid monohydrate / dimethylformamide 4: 85 percent / potassium hydroxide / 2 h / 120 °C View Scheme
参考文献
Sen, Asish K.; Banerji, Nilima
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1989 , vol. 28, # 1-11 p. 818 - 823
反应条件
pyridine; methanol; cyclodextrin glucanotransferase; acetic anhydride; γ-cyclodextrin; BaO; starch Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Ohtani; Aikawa; Fujisawa; Kasai; Tanaka; Yamasaki
Chemical and Pharmaceutical Bulletin, 1991 , vol. 39, # 12 p. 3172 - 3174
反应条件
pyridine; methanol; cyclodextrin glucanotransferase; acetic anhydride; γ-cyclodextrin; BaO; starch Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Ohtani; Aikawa; Fujisawa; Kasai; Tanaka; Yamasaki
Chemical and Pharmaceutical Bulletin, 1991 , vol. 39, # 12 p. 3172 - 3174
反应条件
1: 35 percent / KOH; triethylbenzylammonium chloride / CHCl3; H2O / Heating 2: 62 percent / 1M NaOMe / methanol View Scheme
参考文献
Kariyone et al.
Yakugaku Zasshi, 1958 , vol. 78, p. 939,940
Chem.Abstr., 1958 , p. 20010
反应条件
1: 97 percent / Ag2CO3, H2O / acetone / 16 h / Ambient temperature 2: 84 percent / K2CO3 / CH2Cl2 / 64 h / Ambient temperature View Scheme
参考文献
Abbott, Shaun D.; Gagnon, Lyne; Lagraoui, Mouna; Kadhim, Salam; Attardo, Giorgio; Zacharie, Boulos; Penney, Christopher L.
Journal of Medicinal Chemistry, 1998 , vol. 41, # 11 p. 1909 - 1926
反应条件
silver carbonate in dichloromethane
参考文献
Fujisawa, Takuo; Ichise-Shibuya, Keiko; Katagi, Toshiyuki; Ruzo, Luis O.; Takimoto, Yoshiyuki
Journal of Agricultural and Food Chemistry, 2003 , vol. 51, # 18 p. 5329 - 5336
反应条件
1: silver oxide; diethyl ether 2: barium methylate; methanol View Scheme
参考文献
Noller; Rockwell
Journal of the American Chemical Society, 1938 , vol. 60, p. 2076
反应条件
sodium hydroxide; acetone
参考文献
Velluz; Muller
Bulletin de la Societe Chimique de France, 1955 , p. 198
