乙酰溴-α-D-葡萄糖合成路线 (共 502 条)
反应条件
1: acetone / 18 h / Ambient temperature 2: NaOAc / 100 °C View Scheme
参考文献
Koto, Shinkiti; Yoshida, Toyosaku; Takenaka, Kazuhiro; Zen, Shonosuke
Bulletin of the Chemical Society of Japan, 1982 , vol. 55, # 11 p. 3667 - 3668
反应条件
1: silver oxide; quinoline 2: ammonia; methanol View Scheme
参考文献
Robertson; Waters
Journal of the Chemical Society, 1930 , p. 2729,2732
反应条件
2,2'-azo-bisisobutyronitrile; sodium cyanoborohydride T=80°C; 36 h; Inert atmosphere;
参考文献
Bruyere, Isabelle; Toth, Zoltan; Benyahia, Hamida; Xue, Jia Lu; Praly, Jean-Pierre
Tetrahedron, 2013 , vol. 69, # 46 p. 9656 - 9662
参考文献
Lindberg
Acta Chemica Scandinavica (1947-1973), 1949 , vol. 3, p. 151,152
反应条件
silver nitrate; K22 in N,N-dimethyl-formamide further catalysts, solvents; Product distribution;
参考文献
Audebert, Roland; Quivoron, Claude
Bulletin de la Societe Chimique de France, 1985 , # 6 p. 1107 - 1114
参考文献
Micheel; Baum
Chemische Berichte, 1955 , vol. 88, p. 2020,2024
反应条件
2,6-dimethylpyridine in chloroform T=20°C;
参考文献
Patel, Mitul K.; Vijayakrishnan, Balakumar; Koeppe, Julia R.; Chalker, Justin M.; Doores, Katie J.; Davis, Benjamin G.
Chemical Communications, 2010 , vol. 46, # 48 p. 9119 - 9121
反应条件
1: Ag2CO3 / 4A molecular sieves / CH2Cl2 / 60 h / Ambient temperature 2: K2CO3 / methanol / 4.5 h / Ambient temperature 3: NaH / dimethylformamide / 8 h / Ambient temperature 4: NBS / acetonitrile; H2O / Ambient temperature View Scheme
参考文献
Jansson, Karl; Ahlfors, Stefan; Frejd, Torbjoern; Kihlberg, Jan; Magnusson, Goeran; et al.
Journal of Organic Chemistry, 1988 , vol. 53, # 24 p. 5629 - 5647
反应条件
potassium carbonate 0.5 h; Neat (no solvent)Ball milling;
参考文献
Ramrao Patil, Premanand; Ravindranathan Kartha
Green Chemistry, 2009 , vol. 11, # 7 p. 953 - 956
反应条件
1: diphenyldisulfane With zinc(II) chloride; zinc in acetonitrile T=70°C; 0.75 h; 2: 2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide in acetonitrile T=70°C; 0.416667 h;
参考文献
Mukherjee, Chinmoy; Tiwari, Pallavi; Misra, Anup Kumar
Tetrahedron Letters, 2006 , vol. 47, # 4 p. 441 - 445