乙酰溴-α-D-葡萄糖合成路线 (共 502 条)
反应条件
anhydrous cadmium carbonate in toluene 3 h; Heating;
参考文献
Odinokova, L. E.; Denisenko, M. V.; Denisenko, V. A.; Uvarova, N. I.
Chemistry of Natural Compounds, 1988 , vol. 24, # 2 p. 178 - 183
Khimiya Prirodnykh Soedinenii, 1988 , vol. 24, # 2 p. 212 - 217
反应条件
1: 51.2 percent / silver oxide, quinoline / 20 h / Ambient temperature 2: 98.2 percent / sodium methanolate / methanol / Ambient temperature 3: 94 percent / sodium hydroxide / methanol / 3 h / Ambient temperature View Scheme
参考文献
Grynkiewicz, G.; Achmatowicz, O.; Hennig, J.; Indulski, J.; Klessig, D.F.
Polish Journal of Chemistry, 1993 , vol. 67, # 7 p. 1251 - 1254
反应条件
copper(II) sulfate; mercury dibromide; mercury(II) oxide in chloroform T=0 - 20°C; 10 h;
参考文献
Canadian Journal of Chemistry, , vol. 89, # 8 p. 959 - 963
反应条件
silver carbonate Yield given;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 65, # 12 p. 3257 - 3274
反应条件
pyridine; acetic anhydride 1.) CH2Cl2, reflux, 8 h, 2.) room temperature, 24 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Carbohydrate Research, , vol. 285, p. 159 - 165
反应条件
1: 1.) Ag2O, Drierite / 1.) CH2Cl2, room temperature, 30 min, 2.) CH2Cl2, room temperature, 3 d 2: 80 percent / NaOMe / methanol / 12 h View Scheme
参考文献
Endo, Katsuya; Seya, Kazuhiko; Hikino, Hiroshi
Tetrahedron, 1989 , vol. 45, # 12 p. 3673 - 3682
反应条件
1: benzyl alcohol With silver carbonate in dichloromethane 2 h; Molecular sieveDarknessReflux; 2: 2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide in dichloromethane 24 h; DarknessReflux;
参考文献
Cai, Ji-Bao; Hui, Li; Shen, Xia; Su, Qing-De
Asian Journal of Chemistry, 2010 , vol. 22, # 9 p. 6647 - 6651
反应条件
mercury(II) cyanide in nitromethane
参考文献
Koto, Shinkiti; Morishima, Naohiko; Shichi, Sonoko; Haigoh, Hisamitsu; Hirooka, Motoko; et al.
Bulletin of the Chemical Society of Japan, 1992 , vol. 65, # 12 p. 3257 - 3274
反应条件
silver carbonate in diethyl ether 168 h; Ambient temperaturedarkness;
参考文献
Williams, Patrick J.; Strauss, Christopher R.; Wilson, Bevan; Massy-Westropp, Ralph A.
Phytochemistry (Elsevier), 1983 , vol. 22, # 9 p. 2039 - 2042
反应条件
1: 84 percent / Ag2CO3 2: 67.3 percent / Ag2O / benzene View Scheme
参考文献
Utamura, Toshiko; Kuromatsu, Keiko; Suwa, Kiyoko; Koizumi, Kyoko; Shingu, Tetsuro
Chemical & Pharmaceutical Bulletin, 1986 , vol. 34, p. 2341 - 2353