乙酰溴-α-D-葡萄糖合成路线 (共 502 条)
反应条件
1: Zn; aq. acetic acid / 2.5 h / 0 °C 2: K2CO3 / methanol / 0.67 h View Scheme
参考文献
Witczak, Zbigniew J.; Chen, Hong; Kaplon, Peter
Tetrahedron Asymmetry, 2000 , vol. 11, # 2 p. 519 - 532
反应条件
1: Ag2O; CaSO4 / diethyl ether / 24 h / 20 °C 2: MeONa / methanol / 0.5 h View Scheme
参考文献
Koto, Shinkiti; Morishima, Naohiko; Shichi, Sonoko; Haigoh, Hisamitsu; Hirooka, Motoko; et al.
Bulletin of the Chemical Society of Japan, 1992 , vol. 65, # 12 p. 3257 - 3274
反应条件
1: acetone / 18 h / Ambient temperature 2: NaOAc / 100 °C View Scheme
参考文献
Koto, Shinkiti; Yoshida, Toyosaku; Takenaka, Kazuhiro; Zen, Shonosuke
Bulletin of the Chemical Society of Japan, 1982 , vol. 55, # 11 p. 3667 - 3668
反应条件
trimethylsilylazide; tetrabutyl ammonium fluoride
参考文献
Chinta, Jugun Prakash; Rao, Chebrolu P.
Carbohydrate Research, 2013 , vol. 369, p. 58 - 62
反应条件
potassium carbonate in N,N-dimethyl-formamide T=20°C;
参考文献
Cui, Zining; Yang, Xinling; Shi, Yanxia; Uzawa, Hirotaka; Cui, Jingrong; Dohi, Hirofumi; Nishida, Yoshihiro
Bioorganic and Medicinal Chemistry Letters, 2011 , vol. 21, # 23 p. 7193 - 7196
反应条件
1: 51.2 percent / silver oxide, quinoline / 20 h / Ambient temperature 2: 98.2 percent / sodium methanolate / methanol / Ambient temperature View Scheme
参考文献
Chassagne, David; Crouzet, Jean; Bayonove, Claude L.; Baumes, Raymond L.
Journal of Agricultural and Food Chemistry, 1997 , vol. 45, # 7 p. 2685 - 2689
反应条件
in acetonitrile T=20°C; 3 h;
参考文献
Ollivier; Renaud
Journal of the American Chemical Society, 2001 , vol. 123, # 20 p. 4717 - 4727
反应条件
1: Ag imidazolate, ZnCl2, molecular sieves 2: NaOMe / methanol View Scheme
参考文献
Melvin; McNeill; Henderson; Herbert
Tetrahedron Letters, 1999 , vol. 40, # 6 p. 1201 - 1202
反应条件
1: potassium carbonate; tetrabutylammomium bromide / methanol; water; dichloromethane / 68 h / 20 °C 2: β-glucosidase from almonds; water / aq. phosphate buffer / 0.67 h / 37 °C / pH 7.4 / |Enzymatic reaction View Scheme
参考文献
Oliveri, Valentina; Viale, Maurizio; Caron, Giulia; Aiello, Cinzia; Gangemi, Rosaria; Vecchio, Graziella
Dalton Transactions, 2013 , vol. 42, # 6 p. 2023 - 2034
反应条件
1: Et3N; Bu4NBr / 1,2-dichloro-ethane / 16 h / 75 °C 2: K2CO3 / methanol / 2 h View Scheme
参考文献
Dong, Li; Roosenberg II, John M.; Miller, Marvin J.
Journal of the American Chemical Society, 2002 , vol. 124, # 50 p. 15001 - 15005