乙酰溴-α-D-葡萄糖合成路线 （共 502 条）
反应条件
Ag(1+)*C22H24AgN4(1+)*2Cl(1-) in acetonitrile T=25°C; 3 h; Darkness; stereoselective reaction;
参考文献
Talisman, Ian J.; Kumar, Vineet; Deschamps, Jeffrey R.; Frisch, Mark; Malhotra, Sanjay V.
Carbohydrate Research, 2011 , vol. 346, # 15 p. 2337 - 2341
反应条件
(benzyl)-tri-(butyl)-ammonium chloride; potassium carbonate in chloroform T=20°C; glycosylation;
参考文献
Hongu, Mitsuya; Saito, Kunio; Tsujihara, Kenji
Synthetic Communications, 1999 , vol. 29, # 16 p. 2775 - 2781
反应条件
pyridine; acetic anhydride 1.) CH2Cl2, reflux, 4 h, 2.) room temperature, 24 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Gurudutt, Kambadoor N.; Rao, Lingamallu Jagan Mohan; Rao, Sanjay; Srinivas, Subramanian
Carbohydrate Research, 1996 , vol. 285, p. 159 - 165
反应条件
1: silver oxide; quinoline 2: aqueous KOH-solution View Scheme
参考文献
Muehlemann
Pharmaceutica Acta Helvetiae, 1949 , vol. 24, p. 315,320
反应条件
in acetone 18 h; Ambient temperature;
参考文献
Koto, Shinkiti; Yoshida, Toyosaku; Takenaka, Kazuhiro; Zen, Shonosuke
Bulletin of the Chemical Society of Japan, 1982 , vol. 55, # 11 p. 3667 - 3668
反应条件
iodine; silver carbonate; benzene anschl. mit Natriummethylat in Methanol, danach Erhitzen mit wss. Oxalsaeure;
参考文献
Matsuda; Sekiguchi
Nippon Nogei Kagaku Kaishi, 1959 , vol. 33, p. 309,312
Chem.Abstr., 1963 , vol. 58, p. 5774
Full Text Show Details
Matsuda; Sekiguchi
Tohoku J. agric. Res., 1958 , vol. 9, p. 263,265, 267
反应条件
nitromethane; mercury(II) cyanide anschl. mit Natriummethylat in Methanol;
参考文献
Matsuda
Nippon Nogei Kagaku Kaishi, 1959 , vol. 33, p. 1156
Chem.Abstr., 1963 , vol. 59, p. 6495
Full Text Show Details
Matsuda
Chemistry and Industry (London, United Kingdom), 1958 , p. 1627
反应条件
anschliessende Hydrolyse mit methanol.HCl;
参考文献
Visser et al.
Journal of the American Chemical Society, 1948 , vol. 70, p. 1926
反应条件
pyridine; acetic anhydride 1.) CH2Cl2, reflux, 2 h, 2.) room temperature, 24 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Gurudutt, Kambadoor N.; Rao, Lingamallu Jagan Mohan; Rao, Sanjay; Srinivas, Subramanian
Carbohydrate Research, 1996 , vol. 285, p. 159 - 165
反应条件
(benzyl)-tri-(butyl)-ammonium chloride; potassium carbonate in chloroform T=20°C; glycosylation;
参考文献
Hongu, Mitsuya; Saito, Kunio; Tsujihara, Kenji
Synthetic Communications, 1999 , vol. 29, # 16 p. 2775 - 2781
