乙酰溴-α-D-葡萄糖合成路线 （共 502 条）
参考文献
Hirohara, Shiho; Obata, Makoto; Saito, Atsuhiro; Ogata, Shin-Ichi; Ohtsuki, Chikara; Higashida, Suguru; Ogura, Shun-Ichiro; Okura, Ichiro; Sugai, Yuko; Mikata, Yuji; Tanihara, Masao; Yano, Shigenobu
Photochemistry and Photobiology, 2004 , vol. 80, # 2 p. 301 - 308
反应条件
sodium hydroxide; tetrabutylammomium bromide in chloroform 3 h; Heating;
参考文献
Jain, S. M.; Devi, Sunita; Bani, S.; Singh, Surjit; Singh, G. B.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1988 , vol. 27, # 1-12 p. 1019 - 1023
参考文献
Fox et al.
Journal of the American Chemical Society, 1957 , vol. 79, p. 5060,5062
反应条件
1: silver carbonate 2: sodium methylate; methanol View Scheme
参考文献
Veibel; Eriksen
Bulletin de la Societe Chimique de France, 1936 , vol. <5> 3, p. 277,281
反应条件
silver trifluoroacetate in solid 48 h; Ambient temperature;
参考文献
Im, Juwon; Kim, Jaechul; Kim, Sukjin; Hahn, Bosup; Toda, Fumio
Tetrahedron Letters, 1997 , vol. 38, # 3 p. 451 - 452
反应条件
1: acetonitrile / 0.17 h / Heating 2: 78 percent / Et3N / acetonitrile / 0.17 h / 20 °C View Scheme
参考文献
Ibatullin; Selivanov; Shavva
Synthesis, 2001 , # 3 p. 419 - 422
反应条件
2: ethanolic HCl View Scheme
参考文献
Hilbert; Johnson
Journal of the American Chemical Society, 1930 , vol. 52, p. 4489,4493
反应条件
1: 1.) mercury(II) oxide, mercury(II) bromide, calcium sulfate / 1.) dichloromethane, RT, 30 min 2: 64 percent / m-chloroperbenzoic acid, 2,6-di-t-butyl-4-methylphenol / CH2Cl2 / 4 h / Heating 3: 79 mg / sodium methoxide / methanol / 0.5 h View Scheme
参考文献
Rodriguez, Evelyn B.; Stick, Robert V.
Australian Journal of Chemistry, 1990 , vol. 43, # 4 p. 665 - 679
反应条件
1: o-hydroxynitrobenzene With 1-n-butyl-3-methylimidazolium chloride; silver(l) oxide T=25°C; Koenigs-Knorr type coupling; 0.25 h; Darknessneat (no solvent); 2: 2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide T=25 - 80°C; Koenigs-Knorr type coupling; 0.5 h; Darknessneat (no solvent); optical yield given as percent destereoselective reaction;
参考文献
Kumar, Vineet; Talisman, Ian Jamie; Malhotra, Sanjay V.
European Journal of Organic Chemistry, 2010 , # 18 p. 3377 - 3381
反应条件
1: Ag2CO3 / 4A molecular sieves / CH2Cl2 / 60 h / Ambient temperature 2: K2CO3 / methanol / 4.5 h / Ambient temperature View Scheme
参考文献
Koto, Shinkiti; Morishima, Naohiko; Shichi, Sonoko; Haigoh, Hisamitsu; Hirooka, Motoko; et al.
Bulletin of the Chemical Society of Japan, 1992 , vol. 65, # 12 p. 3257 - 3274
