乙酰溴-α-D-葡萄糖合成路线 （共 502 条）
反应条件
sodium tetrahydroborate; 2,2'-azo-bisisobutyronitrile in acetonitrile
T=80°C; 5 h; Inert atmosphere;
参考文献
Bruyere, Isabelle; Toth, Zoltan; Benyahia, Hamida; Xue, Jia Lu; Praly, Jean-Pierre
Tetrahedron, 2013 , vol. 69, # 46 p. 9656 - 9662
反应条件
2,2'-azo-bisisobutyronitrile; sodium cyanoborohydride
T=80°C; 36 h; Inert atmosphere;
参考文献
Bruyere, Isabelle; Toth, Zoltan; Benyahia, Hamida; Xue, Jia Lu; Praly, Jean-Pierre
Tetrahedron, 2013 , vol. 69, # 46 p. 9656 - 9662
反应条件
AcrH(+)I(-); sodium cyanoborohydride in tetrahydrofuran
1.83333 h; UV-irradiation;
参考文献
Bruyere, Isabelle; Toth, Zoltan; Benyahia, Hamida; Xue, Jia Lu; Praly, Jean-Pierre
Tetrahedron, 2013 , vol. 69, # 46 p. 9656 - 9662
反应条件
AcrH(+)I(-); sodium cyanoborohydride in tert-butyl alcohol
6.5 h; UV-irradiation; Overall yield = 74 percent;
参考文献
Bruyere, Isabelle; Toth, Zoltan; Benyahia, Hamida; Xue, Jia Lu; Praly, Jean-Pierre
Tetrahedron, 2013 , vol. 69, # 46 p. 9656 - 9662
反应条件
2,2'-azo-bisisobutyronitrile; tributyltin chloride; sodium cyanoborohydride in tert-butyl alcohol
T=30 - 35°C; 0.833333 h; Irradiation;
参考文献
Praly, Jean-Pierre; Ardakani, Azin Salek; Bruyere, Isabelle; Marie-Luce, Chrystelle; Bing Qin, Bing
Carbohydrate Research, 2002 , vol. 337, # 18 p. 1623 - 1632
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in toluene
T=110°C; 0.0833333 h; Inert atmosphere; optical yield given as percent de;
参考文献
Lu, Yin-Suo; Li, Qin; Zhang, Li-He; Ye, Xin-Shan
Organic Letters, 2008 , vol. 10, # 16 p. 3445 - 3448
反应条件
azobisisobutyronitrile; tri-n-butyl-tin hydride in toluene
Heating;
参考文献
Bimwala, R. Mampuya; Vogel, Pierre
Journal of Organic Chemistry, 1992 , vol. 57, # 7 p. 2076 - 2083
反应条件
samarium diiodide in tetrahydrofuran
Ambient temperatureslow addition of SmI2; Yield given;
参考文献
Doisneau, Gilles; Beau, Jean-Marie
Tetrahedron Letters, 1998 , vol. 39, # 21 p. 3477 - 3480
反应条件
azobisisobutyronitrile; tri-n-butyl-tin hydride in toluene
1 h; Heating;
参考文献
Bimwala, R. Mampuya; Vogel, Pierre
Journal of Organic Chemistry, 1992 , vol. 57, # 7 p. 2076 - 2083
反应条件
1,1,1,2,2,2-hexabutyl-distannane; 4-methoxy-phenol in benzene
8 h; Ambient temperatureIrradiation; Further byproducts given;
参考文献
Alberti, Angelo; Della Bona, Maria A.; Macciantelli, Dante; Pelizzoni, Francesca; Sello, Guido; Torri, Giangiacomo; Vismara, Elena
Tetrahedron, 1996 , vol. 52, # 30 p. 10241 - 10248
