乙酰溴-α-D-葡萄糖合成路线 (共 502 条)
反应条件
phenol
8 h; Ambient temperatureIrradiation;
参考文献
Alberti, Angelo; Della Bona, Maria A.; Macciantelli, Dante; Pelizzoni, Francesca; Sello, Guido; Torri, Giangiacomo; Vismara, Elena
Tetrahedron, 1996 , vol. 52, # 30 p. 10241 - 10248
反应条件
1: 84 percent / HgO, HgBr2, CaSO4 / CHCl3 / 48 h / Ambient temperature
2: 90 percent / CH3ONa / methanol / 3 h
3: CF3COONa / 0.25 h / Heating
4: BF3*Et2O / toluene / 3 h / 55 °C
5: NaHCO3 / methanol
View Scheme
参考文献
Jansson, Karl; Ahlfors, Stefan; Frejd, Torbjoern; Kihlberg, Jan; Magnusson, Goeran; et al.
Journal of Organic Chemistry, 1988 , vol. 53, # 24 p. 5629 - 5647
反应条件
1: 32 percent / benzyltriethylammonium bromide; NaOH / CHCl3; H2O / 10 h / 60 °C
2: sodium methoxide / methanol / 2 h / 20 °C
View Scheme
参考文献
Orsini, Fulvia; Pelizzoni, Francesca; Bellini, Barbara; Miglierini, Giuliana
Carbohydrate Research, 1997 , vol. 301, # 3-4 p. 95 - 109
反应条件
potassium hydroxide; acetone
参考文献
Merz; Preuss
Archiv der Pharmazie (Weinheim, Germany), 1941 , vol. 279, p. 134,139
Archiv der Pharmazie (Weinheim, Germany), 1943 , vol. 281, p. 205
参考文献
Baba, Naomichi; Makino, Taketoshi; Oda, Jun'ichi; Inouye, Yuzo
Canadian Journal of Chemistry, 1980 , vol. 58, p. 387 - 392
反应条件
1: acetone; potassium carbonate
2: Raney nickel; methanol / Hydrogenation
3: sodium methylate; methanol
View Scheme
参考文献
Latham et al.
Journal of Organic Chemistry, 1950 , vol. 15, p. 884,886
反应条件
potassium hydroxide; water; acetone
参考文献
Robertson
Journal of the Chemical Society, 1927 , p. 1937,1942
反应条件
tetrabutylammomium bromide; sodium hydroxide in dichloromethane
T=40°C; 4 h;
参考文献
Wang, Chao; Zhang, Tian-Tai; Du, Guan-Hua; Zhang, Dong-Ming
Journal of Asian Natural Products Research, 2011 , vol. 13, # 9 p. 817 - 825
反应条件
sodium hydroxide in tetrahydrofuran; acetone
Ambient temperature;
参考文献
Foye; Tovivich
Journal of Pharmaceutical Sciences, 1977 , vol. 66, # 11 p. 1607 - 1611
反应条件
sodium hydroxide in tetrahydrofuran; acetone
Ambient temperature;
参考文献
Foye; Tovivich
Journal of Pharmaceutical Sciences, 1977 , vol. 66, # 11 p. 1607 - 1611