乙酰溴-α-D-葡萄糖合成路线 (共 502 条)
反应条件
sodium hydroxide in tetrahydrofuran; acetone
Ambient temperature;
参考文献
Foye; Tovivich
Journal of Pharmaceutical Sciences, 1977 , vol. 66, # 11 p. 1607 - 1611
反应条件
sodium hydroxide in tetrahydrofuran; acetone
Ambient temperature;
参考文献
Foye; Tovivich
Journal of Pharmaceutical Sciences, 1977 , vol. 66, # 11 p. 1607 - 1611
反应条件
1: aq. NaOH / acetone; tetrahydrofuran / Ambient temperature
2: aq. HCl / methanol / Ambient temperature
View Scheme
参考文献
Foye; Tovivich
Journal of Pharmaceutical Sciences, 1977 , vol. 66, # 11 p. 1607 - 1611
反应条件
1: aq. NaOH / acetone; tetrahydrofuran / Ambient temperature
2: aq. HCl / methanol / Ambient temperature
View Scheme
参考文献
Foye; Tovivich
Journal of Pharmaceutical Sciences, 1977 , vol. 66, # 11 p. 1607 - 1611
反应条件
1: aq. NaOH / acetone; tetrahydrofuran / Ambient temperature
2: aq. HCl / methanol / Ambient temperature
View Scheme
参考文献
Foye; Tovivich
Journal of Pharmaceutical Sciences, 1977 , vol. 66, # 11 p. 1607 - 1611
反应条件
sodium hydroxide in tetrahydrofuran; acetone
Ambient temperature;
参考文献
Foye; Tovivich
Journal of Pharmaceutical Sciences, 1977 , vol. 66, # 11 p. 1607 - 1611
反应条件
1: chloroform; silver oxide; iodine / Reagens 4: Calciumsulfat
2: aqueous acetic acid
View Scheme
参考文献
Haskins et al.
Journal of the American Chemical Society, 1941 , vol. 63, p. 1724
反应条件
bis(1,5-cyclooctadiene)nickel (0); NH4Br; (R,R)-Ph-pybox; zinc in N,N-dimethyl acetamide
T=25°C; 12 h; Inert atmosphere;
参考文献
Gong, Hegui; Andrews, R. Stephen; Zuccarello, Joseph L.; Lee, Stephen J.; Gagne, Michel R.
Organic Letters, 2009 , vol. 11, # 4 p. 879 - 882
反应条件
1: 47.2 percent / Hg(CN)2 / nitromethane; benzene / 3.5 h / 80 °C
2: 83.2 percent / 0.5N NaOH / methanol; CHCl3 / 0.33 h / Ambient temperature
3: 71.4 percent / 1M (n-Bu)4NF / tetrahydrofuran / 20 h / Ambient temperature
View Scheme
参考文献
Mori, Kenji; Funaki, Yuji
Tetrahedron, 1985 , vol. 41, # 12 p. 2379 - 2386
反应条件
1: zinc; ammonium chloride; VO(salen) / methanol
2: sodium methoxide / methanol
3: imidazole / dimethylformamide
View Scheme
参考文献
Stick, Robert V.; Stubbs, Keith A.
Journal of Carbohydrate Chemistry, 2005 , vol. 24, # 4-6 p. 529 - 547