乙酰溴-α-D-葡萄糖合成路线 （共 502 条）
反应条件
1: silver carbonate
2: barium methylate; methanol
View Scheme
参考文献
Compton
Contributions from Boyce Thompson Institute, 1939 , vol. 11, p. 21
反应条件
indium(III) chloride; 4 A molecular sieve in dichloromethane
T=0 - 3°C; 72 h;
参考文献
Ghosh, Rina; Chakraborty, Arijit; Maiti, Dilip K.; Maiti, Swaraj B.
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2002 , vol. 41, # 3 p. 583 - 585
反应条件
1: acetone; aq. NaOH solution
2: methanol. NaOH-solution
View Scheme
参考文献
Robertson; Waters
Journal of the Chemical Society, 1929 , p. 2239,2241
反应条件
potassium fluoride; water; O,O'-bistributyltin benzopinacolate
1.) benzene, 80 deg C, 8 h; 2.) benzene/ether/water, room temp., 1 h; Yield given. Multistep reaction;
参考文献
Hart, David J.; Krishnamurthy, Ramanarayanan; Pook, Lori M.; Seely, Franklin L.
Tetrahedron Letters, 1993 , vol. 34, # 49 p. 7819 - 7822
参考文献
Hilbert; Johnson
Journal of the American Chemical Society, 1930 , vol. 52, p. 4489,4493
反应条件
1: 86 percent / potassium carbonate / acetone; toluene / 1 h
2: NaOMe / methanol
3: mercuric nitrate / acetonitrile
View Scheme
参考文献
Ackermann, Irmtraud E.; Banthorpe, Derek V.; Fordham, William D.; Kinder, John P.; Poots, Ian
Liebigs Annalen der Chemie, 1989 , p. 79 - 82
反应条件
2: 1M CH3ONa / acetic acid / Ambient temperature
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参考文献
Delay, Didier; Delmotte, Francis
Carbohydrate Research, 1990 , vol. 198, # 2 p. 223 - 234
反应条件
potassium hydroxide; chloroform
参考文献
Montgomery et al.
Journal of Organic Chemistry, 1946 , vol. 11, p. 301,305
反应条件
1: 81 percent
2: 5percent aq. KOH / acetone / 0.25 h / Heating
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参考文献
Mezey-Vandor, Gabriella; Farkas, Lorand; Kanzel, Ida; Nogradi, Mihaly
Chemische Berichte, 1980 , vol. 113, # 5 p. 1945 - 1949
反应条件
1: aq. CuSO4; Zn; NaOAc / acetic acid / 2 h / 20 °C
2: Et3N / H2O; methanol / 8 h / 20 °C
3: CuSO4; 4 Angstroem sieves / tetrahydrofuran / 6 h / Heating
View Scheme
参考文献
Witczak, Zbigniew J.; Chen, Hong; Kaplon, Peter
Tetrahedron Asymmetry, 2000 , vol. 11, # 2 p. 519 - 532
