乙酰溴-α-D-葡萄糖合成路线 （共 502 条）
反应条件
1: tetrahydrofuran / 0 - 20 °C / Inert atmosphere
2: acetic anhydride; copper(II) nitrate / 3 h / 105 °C
3: chloroform / 0.5 h / UV-irradiation
View Scheme
参考文献
Kohri, Michinari; Kimura, Takuma; Shinoda, Yoshihiro; Taniguchi, Tatsuo; Nakahira, Takayuki
Carbohydrate Research, 2011 , vol. 346, # 18 p. 2965 - 2969
反应条件
Yield given. Multistep reaction;
参考文献
Delay, Didier; Delmotte, Francis
Carbohydrate Research, 1990 , vol. 198, # 2 p. 223 - 234
反应条件
potassium fluoride; water; O,O'-bistributyltin benzopinacolate
1.) benzene, 80 deg C, 8 h; 2.) benzene/ether/water, room temp., 1 h; Yield given. Multistep reaction;
参考文献
Hart, David J.; Krishnamurthy, Ramanarayanan; Pook, Lori M.; Seely, Franklin L.
Tetrahedron Letters, 1993 , vol. 34, # 49 p. 7819 - 7822
反应条件
1: chloroform; ethanolic KOH-solution
2: pyridine
View Scheme
参考文献
Montgomery et al.
Journal of Organic Chemistry, 1946 , vol. 11, p. 301,305
反应条件
1: Ag2O, I2, CaSO4 / CHCl3 / 18 h
2: NaOMe
View Scheme
参考文献
Namba, Yukihiro; Sakakibara, Toshiyuki; Masada, Mikio; Ito, Fumiaki; Oku, Naoto
Chemistry Letters, 1989 , p. 2145 - 2148
反应条件
1: CaSO4, CF3COOAg, NaHCO3 / diethyl ether / 1 h / 0 °C
2: Amberlyst A-26 / methanol / 3 h / 20 °C
View Scheme
参考文献
Yamahara; Kimura; Kobayashi; Okamoto; Sawada; Fujimura; Chisaka
Chemical and Pharmaceutical Bulletin, 1985 , vol. 33, # 4 p. 1669 - 1675
反应条件
in acetone
T=110°C; 3 h;
参考文献
Sansone, Francesco; Chierici, Elisa; Casnati, Alessandro; Ungaro, Rocco
Organic and biomolecular chemistry, 2003 , vol. 1, # 10 p. 1802 - 1809
反应条件
1: chloroform; ethanolic KOH-solution
2: sodium methylate; methanol
View Scheme
参考文献
Montgomery et al.
Journal of Organic Chemistry, 1946 , vol. 11, p. 301,305
反应条件
chloroform; iodine; silver(l) oxide
Reagens 4: Calciumsulfat;
参考文献
Haskins et al.
Journal of the American Chemical Society, 1941 , vol. 63, p. 1724
反应条件
silver(l) oxide; benzene
参考文献
Richtmyer
Journal of the American Chemical Society, 1934 , vol. 56, p. 1633,1636
