乙酰溴-α-D-葡萄糖合成路线 （共 502 条）
反应条件
1: 86 percent / potassium carbonate / acetone; toluene / 1 h 2: NaOMe / methanol 3: mercuric nitrate / acetonitrile View Scheme
参考文献
Hanessian, Stephen; Bacquet, Christian; Lehong, Nghiep
Carbohydrate Research, 1980 , vol. 80, p. C17 - C22
反应条件
in pyridine; methanol T=80°C; 2.5 h;
参考文献
Wisniewski, Andrzej; Madaj, Janusz; Skorupowa, Eugenia; Sokolowski, Janusz
Journal of Carbohydrate Chemistry, 1994 , vol. 13, # 6 p. 873 - 880
反应条件
1: sodium acetate; CuSO4‵5H2O; zinc; acetic acid / water / 1.5 h / 20 °C 2: TeCl4 / dichloromethane / 0.42 h / 0 - 20 °C / |Inert atmosphere View Scheme
参考文献
Freitas, Juliano C. R.; Couto, Tulio R.; Paulino, Antonio A. S.; Malvestiti, Ivani; Oliveira, Roberta A.; Menezes, Paulo H.; De Freitas Filho, Joao R.
Tetrahedron, 2012 , vol. 68, # 51 p. 10611 - 10620,10
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in 1,2-dichloro-ethane T=-10 - 20°C; 2.5 h;
参考文献
Honda, Ichiro; Shibagaki, Makoto; Koseki, Koshi; Kuno, Hideyuki; Takahashi, Kyoko; Matsushita, Hajime
Heterocycles, 1993 , vol. 36, # 1 p. 149 - 155
反应条件
15-crown-5 in acetonitrile T=20°C; 1 h;
参考文献
Angewandte Chemie - International Edition, , vol. 43, # 23 p. 3069 - 3072
反应条件
sodium tetrahydroborate; 2,2'-azo-bisisobutyronitrile in acetonitrile T=80°C; 5 h; Inert atmosphere;
参考文献
Bruyere, Isabelle; Toth, Zoltan; Benyahia, Hamida; Xue, Jia Lu; Praly, Jean-Pierre
Tetrahedron, 2013 , vol. 69, # 46 p. 9656 - 9662
反应条件
potassium hydroxide in acetonitrile T=20°C; 1 h;
参考文献
Journal of Carbohydrate Chemistry, , vol. 24, # 4-6 p. 649 - 663
反应条件
triethylamine in acetonitrile 48 h; Ambient temperature;
参考文献
Tsvetkov, Yury E.; Byramova, Narguiz E.; Backinowsky, Leon V.
Carbohydrate Research, 1983 , vol. 115, p. 254 - 258
反应条件
potassium tert-butylate in N,N-dimethyl-formamide T=0°C; Koenigs-Knorr glycosidation; 2 h;
参考文献
Chemistry Letters, , vol. 33, # 8 p. 976 - 977
反应条件
potassium hydroxide in acetonitrile T=20°C; 1 h;
参考文献
Journal of Carbohydrate Chemistry, , vol. 24, # 4-6 p. 649 - 663
