乙酰溴-α-D-葡萄糖合成路线 (共 502 条)
反应条件
Beh. der methanol. Loesung des Rktprod. mit wss. HCl;
参考文献
Putman; Hassid
Journal of the American Chemical Society, 1957 , vol. 79, p. 5057,5059
Full Text Show Details
Krahl; Cori
Biochemical Preparations, 1949 , vol. 1, p. 33,36, 40
Full Text Show Details
Cori et al.
Journal of Biological Chemistry, 1937 , vol. 121, p. 465,468, 469
反应条件
water; silver carbonate in acetone 0.5 h;
参考文献
Sabesan; Neira
Carbohydrate Research, 1992 , vol. 223, p. 169 - 185
反应条件
AcrH(+)I(-); sodium cyanoborohydride in acetonitrile T=20°C; 240 h;
参考文献
Bruyere, Isabelle; Toth, Zoltan; Benyahia, Hamida; Xue, Jia Lu; Praly, Jean-Pierre
Tetrahedron, 2013 , vol. 69, # 46 p. 9656 - 9662
反应条件
sodium cyanoborohydride in nitromethane T=100°C; 10.5 h; Inert atmosphere;
参考文献
Bruyere, Isabelle; Toth, Zoltan; Benyahia, Hamida; Xue, Jia Lu; Praly, Jean-Pierre
Tetrahedron, 2013 , vol. 69, # 46 p. 9656 - 9662
反应条件
N,N,N',N'-tetramethyl-urea; silver trifluoromethanesulfonate in various solvent(s) T=25°C; 1.5 h; Yields of byproduct given;
参考文献
Takeo, Ken'ichi
Carbohydrate Research, 1980 , vol. 87, p. 147 - 152
反应条件
sodium cyanoborohydride in tert-butyl alcohol 0.5 h; UV-irradiation;
参考文献
Bruyere, Isabelle; Toth, Zoltan; Benyahia, Hamida; Xue, Jia Lu; Praly, Jean-Pierre
Tetrahedron, 2013 , vol. 69, # 46 p. 9656 - 9662
反应条件
sodium cyanoborohydride in nitromethane T=100°C; 5 h; Inert atmosphere;
参考文献
Bruyere, Isabelle; Toth, Zoltan; Benyahia, Hamida; Xue, Jia Lu; Praly, Jean-Pierre
Tetrahedron, 2013 , vol. 69, # 46 p. 9656 - 9662
反应条件
sodium cyanoborohydride; thiophenol in tert-butyl alcohol 1.75 h; Irradiation;
参考文献
Bruyere, Isabelle; Toth, Zoltan; Benyahia, Hamida; Xue, Jia Lu; Praly, Jean-Pierre
Tetrahedron, 2013 , vol. 69, # 46 p. 9656 - 9662
反应条件
AcrH(+)I(-); sodium cyanoborohydride in tetrahydrofuran 1.83333 h; UV-irradiation;
参考文献
Bruyere, Isabelle; Toth, Zoltan; Benyahia, Hamida; Xue, Jia Lu; Praly, Jean-Pierre
Tetrahedron, 2013 , vol. 69, # 46 p. 9656 - 9662
反应条件
bis(1,5-cyclooctadiene)nickel (0); NH4Br; zinc; Pybox in N,N-dimethyl acetamide T=25°C; 12 h; Inert atmosphere;
参考文献
Gong, Hegui; Andrews, R. Stephen; Zuccarello, Joseph L.; Lee, Stephen J.; Gagne, Michel R.
Organic Letters, 2009 , vol. 11, # 4 p. 879 - 882