5,3'-二羟基-3,7,4'-三甲氧基黄酮合成路线 （共 14 条）
反应条件
1.1: potassium carbonate / N,N-dimethyl-formamide / 10 h / 20 °C / |Inert atmosphere
1.2: 2 h / 80 °C
2.1: potassium carbonate / N,N-dimethyl-formamide / 6 h / 65 °C
3.1: hydrogen; palladium 10 on activated carbon / ethanol; tetrahydrofuran / 1 h / 20 °C / 375.04 Torr
4.1: potassium carbonate / N,N-dimethyl-formamide / 6 h / 65 °C
View Scheme
参考文献
Yamauchi, Kosei; Mitsunaga, Tohru; Inagaki, Mizuho; Suzuki, Tohru
Bioorganic and Medicinal Chemistry, 2014 , vol. 22, # 13 p. 3331 - 3340
反应条件
1: potassium carbonate / N,N-dimethyl-formamide / 6 h / 65 °C
2: hydrogen; palladium 10 on activated carbon / ethanol; tetrahydrofuran / 1 h / 20 °C / 375.04 Torr
3: potassium carbonate / N,N-dimethyl-formamide / 6 h / 65 °C
View Scheme
参考文献
Yamauchi, Kosei; Mitsunaga, Tohru; Inagaki, Mizuho; Suzuki, Tohru
Bioorganic and Medicinal Chemistry, 2014 , vol. 22, # 13 p. 3331 - 3340
反应条件
in 1,4-dioxane
Methylation;
参考文献
Ko, Wun-Chang; Kuo, Shih-Wu; Sheu, Joen-Rong; Lin, Chien-Huang; Tzeng, Shu-Huey; Chen, Chi-Ming
Planta Medica, 1999 , vol. 65, # 3 p. 273 - 275
反应条件
potassium carbonate in N,N-dimethyl-formamide
T=20°C; Product distribution;
参考文献
Bouktaib, Mohamed; Lebrun, Stephane; Atmani, Aziz; Rolando, Christian
Tetrahedron, 2002 , vol. 58, # 50 p. 10001 - 10009
