反应条件
copper(I) bromide in not given Li educt added to CuBr slurry in ether at 0°C under N2, reacted for 10 min, B2H6 soln. added, stirred for 18 h at room temp.; hydrolyzed with H2O, then with aq. NaOH, extd. with ether, aq. phase acidified with aq. HCl, extd. with ether, exts. dried (MgSO4), ether removed, solid recrystd. (petroleum ether);
参考文献
Bullen, N. P.; Chiheru, K. S.; Thorpe, F. G.
Journal of Organometallic Chemistry, 1980 , vol. 195, # 2 p. 147 - 154
