acetophenone oxime carbapalladacycle anchored to SiO2; potassium carbonate in water Suzuki reaction; 48 h; Heating; Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 69, # 2 p. 439 - 446
in tetrahydrofuran; anhydrous butyl ether (under N2); ratio aryl-compd.:Cr(CO)6 1:1, reflux for 48 h in Bu2O-THF; removal of the solvents, sublimation of the residue;
参考文献
Journal of Organometallic Chemistry, , vol. 455, # 1-2 p. 47 - 49
1: toluene / 12 h / |Reflux 2: N-bromosuccinmide / tetrachloromethane / 12 h / |Reflux View Scheme
参考文献
Gorityala, Bala Kishan; Lu, Zhiqiang; Leow, Min Li; Ma, Jimei; Liu, Xue-Wei
Journal of the American Chemical Society, 2012 , vol. 134, # 37 p. 15229 - 15232
Baltus, Christine B.; Press, Neil J.; Antonijevic, Milan D.; Tizzard, Graham J.; Coles, Simon J.; Spencer, John
Tetrahedron, 2012 , vol. 68, # 45 p. 9272 - 9277