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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
2-甲氧基苯基硼酸
合成路线
（共 261 条）
5720-06-9
2-甲氧基苯基硼酸
→
反应条件
920981-16-4
反应条件
1: 30 percent / K2S2O8 / Pd(OAc)2 / acetic acid / 80 °C 2: 82 percent / DBU / benzene / 120 h View Scheme
参考文献
Demchuk, Oleg M.; Yoruk, Bilge; Blackburn, Tom; Snieckus, Victor
Synlett, 2006 , # 18 p. 2908 - 2913
123-56-8
丁二酰亚胺
+
5720-06-9
2-甲氧基苯基硼酸
→
反应条件
92288-64-7
反应条件
pyridine; oxygen; copper diacetate in dichloromethane 168 h;
参考文献
Huegel, Helmut M.; Rix, Colin J.; Fleck, Karin
Synlett, 2006 , # 14 p. 2290 - 2292
106-38-7
对溴甲苯
+
5720-06-9
2-甲氧基苯基硼酸
→
反应条件
92495-53-9
反应条件
K3PO4*3H2O; palladium diacetate in water; dimethylammonium 2,4-dichlorophenoxyacetate T=20°C; Suzuki-Miyaura reaction; 0.5 h;
参考文献
Li, Chen; Li, Xiao-Qiang; Zhang, Chi
Journal of Chemical Research, 2008 , # 9 p. 525 - 527
106-43-4
对氯甲苯
+
5720-06-9
2-甲氧基苯基硼酸
→
反应条件
92495-53-9
反应条件
palladium diacetate; potassium fluoride; biphenyl-2-yl-di-tert-butyl-phosphane in tetrahydrofuran T=20°C; Suzuki coupling; 24 h;
参考文献
Wolfe, John P.; Buchwald, Stephen L.
Angewandte Chemie - International Edition, 1999 , vol. 38, # 16 p. 2413 - 2416
5720-06-9
2-甲氧基苯基硼酸
+
106-49-0
对甲苯胺
→
反应条件
92495-53-9
反应条件
1: p-toluidine With tert.-butylnitrite; boron trifluoride diethyl etherate T=-15 - 5°C; 0.583333 h; 2: 2-Methoxyphenyl-dihydroxyborane With (R,R)-N,N'-(2-MeC6H4)2-N,N'-(cyclohexane-1,2-diyl)thiourea; palladium diacetate in methanol T=20°C; Suzuki reaction; 4 h;
参考文献
Dai, Mingji; Liang, Bo; Wang, Cuihua; Chen, Jiahua; Yang, Zhen
Organic Letters, 2004 , vol. 6, # 2 p. 221 - 224
106-43-4
对氯甲苯
+
5720-06-9
2-甲氧基苯基硼酸
+
224311-51-7
2-(二叔丁基膦)联苯
→
反应条件
92495-53-9
反应条件
potassium fluoride; palladium diacetate in tetrahydrofuran
参考文献
Buchwald, Stephen L.; Huang, Xiaohua; Zim, Danilo
Patent: US2004/171833 A1, 2004 ;
5720-06-9
2-甲氧基苯基硼酸
+
1576-35-8
→
反应条件
92495-53-9
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium carbonate in toluene T=80°C; Suzuki Coupling; 4 h; Sealed tube;
参考文献
Li, Yahui; Liu, Wei; Tian, Qingshan; Yang, Qing; Kuang, Chunxiang
European Journal of Organic Chemistry, 2014 , vol. 2014, # 16 p. 3307 - 3312
5720-06-9
2-甲氧基苯基硼酸
→
反应条件
92495-53-9
反应条件
1: 100 percent / aq. NaOH / toluene 2: 79 percent / 1,1'-bis(diphenylphosphino)ferrocene dichloropalladium / toluene / 24 h / Heating View Scheme
参考文献
Cammidge, Andrew N.; Goddard, Victoria H. M.; Gopee, Hemant; Harrison, Nicola L.; Hughes, David L.; Schubert, Christopher J.; Sutton, Benjamin M.; Watts, Gary L.; Whitehead, Andrew J.
Organic Letters, 2006 , vol. 8, # 18 p. 4071 - 4074
5720-06-9
2-甲氧基苯基硼酸
+
90-13-1
→
反应条件
93321-11-0
反应条件
1: 2-Methoxyphenyl-dihydroxyborane With potassium phosphate; N,N-diisopropyl 2-dicyclohexylphosphino-5-(3'-nitrophenyl)benzamide; palladium diacetate in tetrahydrofuran T=23°C; Suzuki-Miyaura cross-coupling; 0.0166667 h; Inert atmosphere; 2: alpha-chloronaphthalene in tetrahydrofuran; water T=23°C; Suzuki-Miyaura cross-coupling; 6 h; Inert atmosphere;
参考文献
Dai, Wei-Min; Li, Yannian; Zhang, Ye; Yue, Congyong; Wu, Jinlong
Chemistry - A European Journal, 2008 , vol. 14, # 18 p. 5538 - 5554
90-11-9
+
5720-06-9
2-甲氧基苯基硼酸
→
反应条件
93321-11-0
反应条件
1,1'-bis(di-tert-butylphosphino)ferrocene palladium dichloride; potassium carbonate in water; acetonitrile T=60°C; Suzuki-Miyaura reaction; Inert atmosphereSealed vessel;
参考文献
Moseley, Jonathan D.; Murray, Paul M.; Turp, Edward R.; Tyler, Simon N.G.; Burn, Ross T.
Tetrahedron, 2012 , vol. 68, # 30 p. 6010 - 6017
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