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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
2-甲氧基苯基硼酸
合成路线
（共 261 条）
5720-06-9
2-甲氧基苯基硼酸
+
100-01-6
对硝基苯胺
→
反应条件
6460-91-9
反应条件
1: 4-nitro-aniline With tert.-butylnitrite; boron trifluoride diethyl etherate T=-15 - 5°C; 0.583333 h; 2: 2-Methoxyphenyl-dihydroxyborane With (R,R)-N,N'-(2-MeC6H4)2-N,N'-(cyclohexane-1,2-diyl)thiourea; palladium diacetate in methanol T=20°C; Suzuki reaction; 4 h;
参考文献
Dai, Mingji; Liang, Bo; Wang, Cuihua; Chen, Jiahua; Yang, Zhen
Organic Letters, 2004 , vol. 6, # 2 p. 221 - 224
5720-06-9
2-甲氧基苯基硼酸
+
100-00-5
对硝基氯苯
→
反应条件
6460-91-9
反应条件
palladium diacetate; potassium carbonate in ethanol; N,N-dimethyl acetamide T=80°C; Suzuki coupling; 0.5 h;
参考文献
Yang, Weibo; Liu, Chun; Qiu, Jieshan
Chemical Communications, 2010 , vol. 46, # 15 p. 2659 - 2661
636-98-6
4-硝基碘苯
+
5720-06-9
2-甲氧基苯基硼酸
→
反应条件
6460-91-9
反应条件
caesium carbonate; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran Suzuki cross-coupling reaction; Heating;
参考文献
Slegt, Micha; Overkleeft, Hermen S.; Lodder, Gerrit
European Journal of Organic Chemistry, 2007 , # 32 p. 5364 - 5375
5720-06-9
2-甲氧基苯基硼酸
→
反应条件
6460-91-9
反应条件
1: MgSO4 / CH2Cl2 / 20 °C 2: 93 percent / Na2CO3 / Pd/C / H2O; ethanol / 1 h / 20 °C View Scheme
参考文献
Kitamura, Yoshiaki; Sakurai, Ai; Udzu, Takahiro; Maegawa, Tomohiro; Monguchi, Yasunari; Sajiki, Hironao
Tetrahedron, 2007 , vol. 63, # 43 p. 10596 - 10602
609-73-4
2-硝基碘苯
+
5720-06-9
2-甲氧基苯基硼酸
→
反应条件
6460-92-0
反应条件
potassium carbonate; palladium diacetate in methanol; water T=20°C; Suzuki cross-coupling; 28 h;
参考文献
Gonzalez, Raquel Rodriguez; Liguori, Lucia; Carrillo, Alberto Martinez; Bjorsvik, Hans-Rene
Journal of Organic Chemistry, 2005 , vol. 70, # 23 p. 9591 - 9594
5720-06-9
2-甲氧基苯基硼酸
+
88-73-3
邻氯硝基苯
→
反应条件
6460-92-0
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium carbonate in water; N,N-dimethyl-formamide Suzuki-Miyaura coupling; 0.25 h; Inert atmosphereMicrowave irradiation;
参考文献
Peng, Haixia; Chen, Xuxing; Chen, Yanhong; He, Qian; Xie, Yuyuan; Yang, Chunhao
Tetrahedron, 2011 , vol. 67, # 32 p. 5725 - 5731
5720-06-9
2-甲氧基苯基硼酸
+
365-33-3
2-硝基重氮苯四氟硼酸盐
→
反应条件
6460-92-0
反应条件
palladium diacetate in 1,4-dioxane T=20°C; Suzuki-Miyamura cross-coupling; chemoselective reaction;
参考文献
Kuethe, Jeffrey T.; Childers, Karla G.
Advanced Synthesis and Catalysis, 2008 , vol. 350, # 10 p. 1577 - 1586
609-73-4
2-硝基碘苯
+
5720-06-9
2-甲氧基苯基硼酸
→
反应条件
6460-92-0
+
4877-93-4
2,2’-二甲氧基联苯
反应条件
potassium dihydrogenphosphate; tetrabutylammomium bromide; palladium diacetate in water; N,N-dimethyl-formamide T=100°C; Suzuki cross-coupling;
参考文献
Gonzalez, Raquel Rodriguez; Liguori, Lucia; Carrillo, Alberto Martinez; Bjorsvik, Hans-Rene
Journal of Organic Chemistry, 2005 , vol. 70, # 23 p. 9591 - 9594
577-19-5
1-溴-2-硝基苯
+
5720-06-9
2-甲氧基苯基硼酸
→
反应条件
6460-92-0
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium carbonate Suzuki coupling;
参考文献
Mu, Hong-Liang; Ye, Wei-Ping; Song, Dong-Po; Li, Yue-Sheng
Organometallics, 2010 , vol. 29, # 23 p. 6282 - 6290
1428743-71-8
+
5720-06-9
2-甲氧基苯基硼酸
→
反应条件
646522-93-2
反应条件
1: 2,5-dioxotetrahydro-1H-1-pyrrolyl 3,7-dimethyl-6-octenoate With palladium diacetate; sodium carbonate; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=60°C; Inert atmosphere; 2: 2-Methoxyphenyl-dihydroxyborane in tetrahydrofuran; water T=25 - 60°C; Inert atmosphere;
参考文献
Kapdi, Anant R.; Fairlamb, Ian J. S.
New Journal of Chemistry, 2013 , vol. 37, # 4 p. 961 - 964
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