反应条件
mercury(II) diacetate in chloroform addn. of B-compd. to stirred mixt. of Pb-compd. and Hg-compd. in CHCl3 over 15 min (40°C), stirring (40°C, 1 h and room temp. overnight); filtration (Celite), concn. (40°C), addn. of petroleum ether, standing (0°C, overnight), stirring in mixt. of acetic acid and CHCl3, washing (H2O), drying (Na2SO4), concn., addn. of petroleum ether, crystn. (0°C);
参考文献
Morgan, Jacqueline; Pinhey, John T.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , p. 715 - 720
