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乙二醇
甲醛
63148-62-9
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丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-甲氧基苯硼酸
合成路线
（共 1108 条）
1119-64-8
+
5720-07-0
4-甲氧基苯硼酸
→
反应条件
131558-77-5
反应条件
copper(l) iodide; 8-hydroxy-quinoline; sodium salt of phosphorous acid in ethanol T=80°C; Suzuki coupling; 24 h;
参考文献
Wang, Shihua; Wang, Min; Wang, Lei; Wang, Bo; Li, Pinhua; Yang, Jin
Tetrahedron, 2011 , vol. 67, # 26 p. 4800 - 4806
5720-07-0
4-甲氧基苯硼酸
→
反应条件
131558-77-5
反应条件
copper(l) iodide; potassium carbonate in ethylene glycol dimethyl ether; N,N-dimethyl-formamide T=20°C; 1 h;
参考文献
Yu, Chan-Mo; Kweon, Jae-Hong; Ho, Pil-Su; Kang, Sin-Cheol; Lee, Gong Yeal
Synlett, 2005 , # 17 art. no. U23005ST, p. 2631 - 2634
3017-70-7
2-溴-3-甲基-2-丁烯
+
5720-07-0
4-甲氧基苯硼酸
→
反应条件
13399-33-2
反应条件
bis(η3-allyl-μ-chloropalladium(II)); Tedicyp; potassium carbonate in N,N-dimethyl-formamide T=100°C; Suzuki cross-coupling; 20 h;
参考文献
Berthiol, Florian; Doucet, Henri; Santelli, Maurice
European Journal of Organic Chemistry, 2003 , # 6 p. 1091 - 1096
5720-07-0
4-甲氧基苯硼酸
→
反应条件
13399-33-2
反应条件
1: sodium hydroxide / toluene / 60 °C / Inert atmosphere 2: Pd/N-heterocyclic carbene View Scheme
参考文献
Schumacher, Andreas; Schrems, Marcus G.; Pfaltz, Andreas
Chemistry - A European Journal, 2011 , vol. 17, # 48 p. 13502 - 13509
5720-07-0
4-甲氧基苯硼酸
+
7065-92-1
→
反应条件
10166-78-6
反应条件
potassium carbonate; tetrakis(triphenylphosphine) palladium(0) in ethanol; toluene Suzuki-Miyaura coupling; 48 h; Heating;
参考文献
Mao, Lisheng; Sakurai, Hidehiro; Hirao, Toshikazu
Synthesis, 2004 , # 15 p. 2535 - 2539
1532-97-4
+
5720-07-0
4-甲氧基苯硼酸
→
反应条件
101273-53-4
反应条件
dichloro[N-hydroxy-1-(1-methyl-1H-benzimidazol-2-yl-κN3)ethanamine-κN]palladium; tetrabutylammomium bromide; potassium hydroxide in water T=160°C; Suzuki coupling; 0.2 h; Microwave irradiation;
参考文献
Arkivoc, , vol. 2010, # 9 p. 319 - 330
91-22-5
+
5720-07-0
4-甲氧基苯硼酸
→
反应条件
16032-40-9
反应条件
1: (4-methoxyphenyl)-boronic acid With diethylzinc in 1,4-dioxane T=60°C; 12 h; 2: quinoline With [Ni0(1,5-cyclooctadiene)2]; tri-cyclo-hexyl-phosphine in 1,4-dioxane; toluene T=130°C; 20 h;
参考文献
Hyodo, Isao; Tobisu, Mamoru; Chatani, Naoto
Chemistry - An Asian Journal, 2012 , vol. 7, # 6 p. 1357 - 1365
→
反应条件
16032-40-9
反应条件
potassium phosphate; [1,3-bis(diphenylphosphino) propane] dichloronickel(II) in 1,4-dioxane T=100 - 110°C; Suzuki coupling; Inert atmosphere;
参考文献
Chen, Guo-Jun; Han, Fu-She
European Journal of Organic Chemistry, 2012 , # 19 p. 3575 - 3579
5720-07-0
4-甲氧基苯硼酸
+
59-31-4
→
反应条件
16032-40-9
反应条件
1: 2-hydroxyquinoline With potassium carbonate; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate in 1,4-dioxane T=100°C; 3 h; Inert atmosphere; 2: (4-methoxyphenyl)-boronic acid With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in 1,4-dioxane; water T=100°C; Suzuki-Miyaura coupling; Inert atmosphere;
参考文献
Li, Shui-Ming; Huang, Jie; Chen, Guo-Jun; Han, Fu-She
Chemical Communications, 2011 , vol. 47, # 48 p. 12840 - 12842
871507-79-8
+
5720-07-0
4-甲氧基苯硼酸
→
反应条件
16032-40-9
+
1106785-14-1
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium carbonate in ethanol; water; toluene Suzuki coupling; 24 h; RefluxInert atmosphere;
参考文献
Lord, Anna-Marie; Mahon, Mary F.; Lloyd, Matthew D.; Threadgill, Michael D.
Journal of Medicinal Chemistry, 2009 , vol. 52, # 3 p. 868 - 877
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