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乙二醇
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63148-62-9
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二甲基亚砜
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471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-甲氧基苯硼酸
合成路线
（共 1108 条）
66950-63-8
+
5720-07-0
4-甲氧基苯硼酸
→
反应条件
613-37-6
4-甲氧基联苯
反应条件
morpholine; C31H45Cl2N3OPd; caesium carbonate in water T=110°C; Suzuki-Miyaura Coupling; 12 h; Inert atmosphere;
参考文献
Wang, Zhan-Yong; Ma, Qin-Na; Li, Ren-Hao; Shao, Li-Xiong
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 45 p. 7899 - 7906
5720-07-0
4-甲氧基苯硼酸
+
100-63-0
苯肼
→
反应条件
613-37-6
4-甲氧基联苯
反应条件
bis-triphenylphosphine-palladium(II) chloride; sodium lauryl sulfate; potassium carbonate; p-toluenesulfonyl chloride in water T=60°C; Suzuki Coupling;
参考文献
Liu, Jin-Biao; Zhou, He-Ping; Peng, Yi-Yuan
Tetrahedron Letters, 2014 , vol. 55, # 17 p. 2872 - 2875
5720-07-0
4-甲氧基苯硼酸
+
369-57-3
四氟硼酸重氮苯盐
→
反应条件
613-37-6
4-甲氧基联苯
反应条件
SIDip*HCl; palladium diacetate in tetrahydrofuran T=0°C; Sizuki-Miyaura cross coupling; 2.5 h;
参考文献
Andrus; Song
Organic letters, 2001 , vol. 3, # 23 p. 3761 - 3764
5720-07-0
4-甲氧基苯硼酸
+
13116-27-3
4-碘苯肼
→
反应条件
613-37-6
4-甲氧基联苯
反应条件
1: para-iodophenyl hydrazine With polystyrene-NHCO(CH2)4COOH; benzotriazol-1-ol; diisopropyl-carbodiimide in dichloromethane Solid phase reaction; 2: (4-methoxyphenyl)-boronic acid With potassium phosphate; tetrakis(triphenylphosphine) palladium(0); water in N,N-dimethyl-formamide T=80°C; Suzuki coupling reaction; 24 h; 3: With propylamine; copper diacetate T=20°C; Oxidation; 2 h;
参考文献
Stieber, Frank; Grether, Uwe; Waldmann, Herbert
Angewandte Chemie - International Edition, 1999 , vol. 38, # 8 p. 1073 - 1077
65009-00-9
苯基二乙基氨基甲酸酯
+
5720-07-0
4-甲氧基苯硼酸
→
反应条件
613-37-6
4-甲氧基联苯
反应条件
1: (4-methoxyphenyl)-boronic acid T=75°C; 4 h; dehydrationvacuum; 2: phenyl diethylcarbamate With potassium phosphate; NiCl2(PCy3)2; PCy3∙HBF4 in o-xylene T=150°C; Suzuki-Miyaura coupling; 5 h; Inert atmosphere;
参考文献
Antoft-Finch, Aurora; Blackburn, Tom; Snieckus, Victor
Journal of the American Chemical Society, 2009 , vol. 131, # 49 p. 17750 - 17752
16156-59-5
+
5720-07-0
4-甲氧基苯硼酸
→
反应条件
613-37-6
4-甲氧基联苯
反应条件
potassium phosphate; zinc; 1,1'-bis(diphenylphosphanyl)ferrocenenickel(II) chloride; potassium iodide in 1,4-dioxane T=100°C; 24 h;
参考文献
Percec, Virgil; Bae, Jin-Young; Hill, Dale H.
Journal of Organic Chemistry, 1995 , vol. 60, # 4 p. 1060 - 1065
5720-07-0
4-甲氧基苯硼酸
+
2001-45-8
→
反应条件
613-37-6
4-甲氧基联苯
反应条件
palladium diacetate; sodium acetate in N,N-dimethyl-formamide T=100°C; Suzuki-Miyaura reaction; 12 h;
参考文献
Hwang, Lee Kyoung; Na, Youngim; Lee, Junseong; Do, Youngkyu; Chang, Sukbok
Angewandte Chemie - International Edition, 2005 , vol. 44, # 38 p. 6166 - 6169
5720-07-0
4-甲氧基苯硼酸
+
183803-06-7
→
反应条件
799766-18-0
+
613-37-6
4-甲氧基联苯
反应条件
sodium carbonate; tetrakis(triphenylphosphine) palladium(0) in ethylene glycol dimethyl ether; water Heating / reflux;
参考文献
WYETH
Patent: WO2004/103941 A2, 2004 ;
Location in patent: Page 29-30 ;
WO 2004/103941 A2
5720-07-0
4-甲氧基苯硼酸
→
反应条件
613-37-6
4-甲氧基联苯
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium carbonate in ethylene glycol dimethyl ether; water 0.5 h; Ambient temperature;
参考文献
Kang, Suk-Ku; Lee, Hong-Woo; Jang, Su-Bum; Ho, Pil-Su
Journal of Organic Chemistry, 1996 , vol. 61, # 14 p. 4720 - 4724
5720-07-0
4-甲氧基苯硼酸
+
3076-54-8
→
反应条件
613-37-6
4-甲氧基联苯
反应条件
sodium methylate; tris(dibenzylideneacetone)dipalladium(0) chloroform complex; copper(l) iodide in ethylene glycol dimethyl ether; acetonitrile T=60°C; 2 h;
参考文献
Kang, Suk-Ku; Ryu, Hyung-Chul; Son, Hoe-Joo
Synlett, 1998 , # 7 p. 771 - 773
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