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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-甲氧基苯硼酸
合成路线
（共 1108 条）
92-66-0
4-溴代联苯
+
5720-07-0
4-甲氧基苯硼酸
→
反应条件
13041-66-2
反应条件
1: (4-methoxyphenyl)-boronic acid With potassium phosphate; 2C2F6NO4S2(1-)*C44H66Cl2N2P2Pd(2+); (BMPL) bis(trifluoromethylsulfonyl)imide in water T=65°C; Suzuki-Miyaura reaction; Inert atmosphere; 2: 4-bromo-1,1'-biphenyl in water T=65°C; Suzuki-Miyaura reaction; 2 h; Inert atmosphere;
参考文献
Lombardo, Marco; Chiarucci, Michel; Trombini, Claudio
Green Chemistry, 2009 , vol. 11, # 4 p. 574 - 579
92-86-4
4,4-二溴联苯
+
5720-07-0
4-甲氧基苯硼酸
→
反应条件
13041-66-2
反应条件
tetrakis(triphenylphosphine) palladium(0); caesium carbonate in methanol; toluene Suzuki-Miyaura cross coupling; 12 h; Inert atmosphereReflux; regiospecific reaction;
参考文献
Guillen, Elena; Hierrezuelo, Jesus; Martinez-Mallorquin, Rocio; Lopez-Romero, J. Manuel; Rico, Rodrigo
Tetrahedron, 2011 , vol. 67, # 14 p. 2555 - 2561
5720-07-0
4-甲氧基苯硼酸
+
2051-62-9
4-氯联苯
→
反应条件
13041-66-2
反应条件
(IPr)Pd(cinnamyl)(Cl); triethylamine in water T=23°C; Suzuki-Miyaura reaction; 8 h; Inert atmosphereMicellar solution;
参考文献
Lipshutz, Bruce H.; Petersen, Tue B.; Abela, Alexander R.
Organic Letters, 2008 , vol. 10, # 7 p. 1333 - 1336
589-87-7
对溴碘苯
+
5720-07-0
4-甲氧基苯硼酸
+
98-80-6
苯硼酸
→
反应条件
13041-66-2
反应条件
1: 4-bromo-1-iodobenzene; 3,4,5-trimethoxyphenylboronic acid With tris-imidazolium-stabilized palladium; potassium carbonate in water; toluene T=40°C; Suzuki coupling; 20 h; 2: (4-methoxyphenyl)-boronic acid in water; toluene T=40°C; Suzuki coupling; 19 h;
参考文献
Planellas, Marc; Pleixats, Roser; Shafir, Alexandr
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 4 p. 651 - 662
5720-07-0
4-甲氧基苯硼酸
→
反应条件
13041-66-2
反应条件
1: 74 percent / aq. sodium carbonate; Pd(PPh3)4 / toluene; ethanol / 6 h / Heating 2: 73 percent / dppfNiCl2 / tetrahydrofuran / 16 h / Heating View Scheme
参考文献
Jo, Hyunjong; Kim, Chul-Bae; Ryoo, Tae-Yong; Ahn, Bo-Kyoung; Park, Kwangyong
Bulletin of the Korean Chemical Society, 2010 , vol. 31, # 12 p. 3749 - 3754
5720-07-0
4-甲氧基苯硼酸
+
583-53-9
1,2-二溴苯
→
反应条件
160538-35-2
反应条件
potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine in tetrahydrofuran T=20°C; Suzuli coupling; 6 h;
参考文献
Dong, Cheng-Guo; Hu, Qiao-Sheng
Journal of the American Chemical Society, 2005 , vol. 127, # 28 p. 10006 - 10007
615-42-9
1,2-二碘苯
+
5720-07-0
4-甲氧基苯硼酸
→
反应条件
160538-35-2
反应条件
sodium hydroxide; tetrakis(triphenylphosphine) palladium(0) in ethylene glycol dimethyl ether T=80°C; Suzuki-Miyaura reaction; 1.2 h;
参考文献
King, Benjamin T.; Kroulik, Jiri; Robertson, Charles R.; Rempala, Pawel; Hilton, Cameron L.; Korinek, Justin D.; Gortari, Lisa M.
Journal of Organic Chemistry, 2007 , vol. 72, # 7 p. 2279 - 2288
5720-07-0
4-甲氧基苯硼酸
+
95-50-1
邻二氯苯
→
反应条件
160538-35-2
反应条件
C28H44N2PPd; potassium carbonate in ethanol; water T=60°C; Suzuki coupling; 5 h;
参考文献
Lee, Dong-Hwan; Jin, Myung-Jong
Organic Letters, 2011 , vol. 13, # 2 p. 252 - 255
5720-07-0
4-甲氧基苯硼酸
+
95-50-1
邻二氯苯
→
反应条件
92023-24-0
+
160538-35-2
反应条件
tris-(dibenzylideneacetone)dipalladium(0); caesium carbonate; tri-cyclo-hexyl-phosphine in toluene T=70°C; Suzuki coupling; Inert atmosphere; chemoselective reaction;
参考文献
Ullah, Ehsan; McNulty, James; Robertson, Al
European Journal of Organic Chemistry, 2012 , # 11 p. 2127 - 2131
5720-07-0
4-甲氧基苯硼酸
+
583-53-9
1,2-二溴苯
→
反应条件
74447-76-0
+
160538-35-2
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium carbonate; triphenylphosphine in tetrahydrofuran; water T=80°C; Suzuki coupling;
参考文献
Dong, Cheng-Guo; Liu, Tao-Ping; Hu, Qiao-Sheng
Synlett, 2009 , # 7 p. 1081 - 1086
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