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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-甲氧基苯硼酸
合成路线
（共 1108 条）
5720-07-0
4-甲氧基苯硼酸
+
24241-18-7
2-氨基-3,5-二溴吡嗪
→
反应条件
174680-63-8
反应条件
bis(benzonitrile)palladium(II) dichloride; sodium carbonate; 1,4-di(diphenylphosphino)-butane in ethanol; toluene 24 h; Heating;
参考文献
Cavalier; Burton; De Tollenaere; Dussart; Marchand; Rees; Marchand-Brynaert
Synthesis, 2001 , # 5 p. 768 - 772
5720-07-0
4-甲氧基苯硼酸
+
90-05-1
愈创木酚
→
反应条件
1655-72-7
1-甲氧基-2-(4-甲氧基苯氧基)苯
反应条件
copper diacetate; 4 A molecular sieve; triethylamine in dichloromethane T=25°C; 18 h;
参考文献
Evans, David A.; Katz, Jeffrey L.; West, Theodore R.
Tetrahedron Letters, 1998 , vol. 39, # 19 p. 2937 - 2940
5720-07-0
4-甲氧基苯硼酸
→
反应条件
1655-74-9
双(4-甲氧基二苯基)醚
反应条件
copper diacetate; water; triethylamine in dichloromethane; acetonitrile T=25°C; 6 h;
参考文献
Sagar; Tale; Adude
Tetrahedron Letters, 2003 , vol. 44, # 37 p. 7061 - 7063
5720-07-0
4-甲氧基苯硼酸
+
105-07-7
4-氰基苯甲醛
→
反应条件
174813-84-4
4-(羟基(4-甲氧基苯基)甲基)苯甲腈
反应条件
potassium phosphate; ferrocenyl-containing palladacycle in toluene T=20°C;
参考文献
He, Ping; Lu, Yong; Dong, Cheng-Guo; Hu, Qiao-Sheng
Organic Letters, 2007 , vol. 9, # 2 p. 343 - 346
6952-59-6
间溴苯腈
+
5720-07-0
4-甲氧基苯硼酸
→
反应条件
154197-00-9
反应条件
potassium phosphate; [5-(3-butylbenzimidazol-2-yliden-1-yl)-25,26,27,28-tetrapropyloxy calix[4]arene] (pyridine) palladium(II) dibromide in 1,4-dioxane T=100°C; 24 h; Inert atmosphere;
参考文献
Ren, Hui; Xu, Yong; Jeanneau, Erwann; Bonnamour, Isabelle; Tu, Tao; Darbost, Ulrich
Tetrahedron, 2014 , vol. 70, # 17 p. 2829 - 2837
873-32-5
邻氯苯腈
+
5720-07-0
4-甲氧基苯硼酸
→
反应条件
154197-00-9
反应条件
tetrabutylammomium bromide; potassium carbonate; star-shaped oxime-palladacycle in N,N-dimethyl-formamide T=110°C; Suzuki coupling; 24 h;
参考文献
Liu, Qing-Ping; Chen, Ying-Chun; Wu, Yong; Zhu, Jin; Deng, Jin-Gen
Synlett, 2006 , # 10 p. 1503 - 1506
585-76-2
3-溴苯甲酸
+
5720-07-0
4-甲氧基苯硼酸
→
反应条件
154197-00-9
反应条件
1: 3-bromophenylacetic acid With resin-bound amine; benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate in N,N-dimethyl-formamide T=20°C; 18 h; 2: (4-methoxyphenyl)-boronic acid With tetrakis(triphenylphosphine) palladium(0); sodium carbonate in ethylene glycol dimethyl ether Suzuki coupling; 48 h; Heating; 3: With pyridine; trifluoroacetic anhydride in dichloromethane T=20°C; 16 h;
参考文献
Hone, Neal D.; Payne, Lloyd J.; Tice, Colin M.
Tetrahedron Letters, 2001 , vol. 42, # 6 p. 1115 - 1118
6952-59-6
间溴苯腈
+
31268-20-9
+
5720-07-0
4-甲氧基苯硼酸
→
反应条件
71426-20-5
+
154197-00-9
反应条件
palladium diacetate; cesium fluoride; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in tetrahydrofuran T=65°C; Suzuki-Miyaura reaction; 5 h; Inert atmosphere;
参考文献
Mollar, Cristian; Besora, Maria; Maseras, Feliu; Asensio, Gregorio; Medio-Simon, Mercedes
Chemistry - A European Journal, 2010 , vol. 16, # 45 p. 13390 - 13397
10075-50-0
5-溴吲哚
+
5720-07-0
4-甲氧基苯硼酸
→
反应条件
144104-46-1
5-(4-甲氧基苯基)-1H-吲哚
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium carbonate in ethanol; toluene Suzuki coupling; 5 h; Heating;
参考文献
Prieto, Monica; Zurita, Esther; Rosa, Esmeralda; Munoz, Lourdes; Lloyd-Williams, Paul; Giralt, Ernest
Journal of Organic Chemistry, 2004 , vol. 69, # 20 p. 6812 - 6820
4774-14-5
2,6-二氯吡嗪
+
5720-07-0
4-甲氧基苯硼酸
→
反应条件
135459-44-8
反应条件
sodium hydrogencarbonate; tetrakis(triphenylphosphine) palladium(0) in ethanol; toluene Suzuki coupling; 14 h; Heating;
参考文献
Dias, Nathalie; Jacquemard, Ulrich; Baldeyrou, Brigitte; Lansiaux, Amelie; Goossens, Jean-Francois; Bailly, Christian; Routier, Sylvain; Merour, Jean-Yves
European Journal of Medicinal Chemistry, 2005 , vol. 40, # 12 p. 1206 - 1213
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