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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-甲氧基苯硼酸
合成路线
（共 1108 条）
5720-07-0
4-甲氧基苯硼酸
+
98-56-6
对氯三氟甲苯
→
反应条件
10355-12-1
反应条件
K3PO4*3H2O; (2-mesityl-1H-inden-3-yl)dicyclohexylphosphine; palladium diacetate; Aliquatreg; 336 in water T=20 - 100°C; Suzuki-Miyaura Coupling; 8 h; Inert atmosphere;
参考文献
Mao, Shu-Lan; Sun, Yue; Yu, Guang-Ao; Zhao, Cui; Han, Zhi-Jun; Yuan, Jia; Zhu, Xiaolei; Yang, Qihua; Liu, Sheng-Hua
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 47 p. 9410 - 9417
5720-07-0
4-甲氧基苯硼酸
→
反应条件
10355-12-1
+
194873-98-8
反应条件
1: 3-chloro-benzenecarboperoxoic acid; boron trifluoride diethyl etherate / diethyl ether; dichloromethane 2: trifluoroacetic acid sodium salt / water; dichloromethane 3: 2Na(1+)*H2O*Cl4Pt(2-); acetic acid; tetrabutylammonium trifluoromethanesulphonate / 72 h View Scheme
参考文献
Wagner, Anna M.; Hickman, Amanda J.; Sanford, Melanie S.
Journal of the American Chemical Society, 2013 , vol. 135, # 42 p. 15710 - 15713
5720-07-0
4-甲氧基苯硼酸
+
99-90-1
4-溴苯乙酮
→
反应条件
13021-18-6
1-(4-甲氧基-联苯-4-基)-乙酮
反应条件
sodium salt of phosphorous acid; palladium on activated charcoal in water; isopropyl alcohol T=20°C; Suzuki-Miyaura reaction; 2 h;
参考文献
Zhang, Guolin
Journal of Chemical Research, 2004 , # 9 p. 593 - 595
5720-07-0
4-甲氧基苯硼酸
+
99-91-2
对氯苯乙酮
→
反应条件
13021-18-6
1-(4-甲氧基-联苯-4-基)-乙酮
反应条件
NHC-Pd(II)-Im; potassium tert-butylate in water T=80°C; Suzuki-Miyaura coupling; 12 h;
参考文献
Zhou, Xia-Xia; Shao, Li-Xiong
Synthesis, 2011 , # 19 art. no. H53711SS, p. 3138 - 3142
13329-40-3
4-碘代苯乙酮
+
5720-07-0
4-甲氧基苯硼酸
→
反应条件
13021-18-6
1-(4-甲氧基-联苯-4-基)-乙酮
反应条件
Cyphos® IL 101; potassium phosphate; tris(dibenzylideneacetone)dipalladium(0) chloroform complex in toluene T=50°C; Suzuki cross-coupling; 1 h;
参考文献
Cano, Rafael; Ramon, Diego J.; Yus, Miguel
Tetrahedron, 2011 , vol. 67, # 30 p. 5432 - 5436
64101-67-3
+
5720-07-0
4-甲氧基苯硼酸
→
反应条件
13021-18-6
1-(4-甲氧基-联苯-4-基)-乙酮
反应条件
anhydrous dipotassium phosphate; [1,3-bis(diphenylphosphino) propane] dichloronickel(II) in 1,4-dioxane T=100 - 110°C; Suzuki-Miyaura coupling reaction; Inert atmosphere;
参考文献
Gao, Han; Li, You; Zhou, Yi-Guo; Han, Fu-She; Lin, Ying-Jie
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 2-3 p. 309 - 314
5720-07-0
4-甲氧基苯硼酸
+
1777-57-7
→
反应条件
13021-18-6
1-(4-甲氧基-联苯-4-基)-乙酮
+
254453-87-7
反应条件
cesium fluoride; tetrakis(triphenylphosphine) palladium(0) in ethylene glycol dimethyl ether T=75°C; Suzuki-Kumada coupling; 3 h;
参考文献
Thiemann, Thies; Umeno, Kuniharu; Wang, Jian; Tabuchi, Yumiko; Arima, Kazuya; Watanabe, Masataka; Tanaka, Yasuko; Gorohmaru, Hideki; Mataka, Shuntaro
Journal of the Chemical Society. Perkin Transactions 1, 2002 , # 18 p. 2090 - 2110
69497-83-2
+
5720-07-0
4-甲氧基苯硼酸
→
反应条件
13021-18-6
1-(4-甲氧基-联苯-4-基)-乙酮
反应条件
anhydrous dipotassium phosphate; [1,3-bis(diphenylphosphino) propane] dichloronickel(II) in 1,4-dioxane T=100 - 110°C; Suzuki-Miyaura coupling reaction; Inert atmosphere;
参考文献
Gao, Han; Li, You; Zhou, Yi-Guo; Han, Fu-She; Lin, Ying-Jie
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 2-3 p. 309 - 314
1432739-32-6
+
5720-07-0
4-甲氧基苯硼酸
→
反应条件
13021-18-6
1-(4-甲氧基-联苯-4-基)-乙酮
反应条件
morpholine; C31H45Cl2N3OPd; caesium carbonate in water T=110°C; Suzuki-Miyaura Coupling; 12 h; Inert atmosphere;
参考文献
Wang, Zhan-Yong; Ma, Qin-Na; Li, Ren-Hao; Shao, Li-Xiong
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 45 p. 7899 - 7906
5720-07-0
4-甲氧基苯硼酸
→
反应条件
13021-18-6
1-(4-甲氧基-联苯-4-基)-乙酮
反应条件
tri-tert-butyl phosphine; boron trifluoride diethyl etherate; tris(dibenzylideneacetone)dipalladium (0) in ethylene glycol dimethyl ether; hexane T=20°C; 1 h;
参考文献
Saeki, Tomoyuki; Son, Eun-Cheol; Tamao, Kohei
Organic Letters, 2004 , vol. 6, # 4 p. 617 - 619
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