10-甲基-1,4-二氧杂螺[4.5]癸-6-烯合成路线 （共 1 条）
反应条件
1: m-chloroperbenzoic acid 2: 93 percent / Zn, chlorotrimethylsilane / CH2Cl2 / 0.5 h / 0 °C 3: 72 percent / pyridine, Cr2O3, kieselguhr / CH2Cl2 / 0.33 h / Ambient temperature 4: 65 percent / silica gel, 15percent H2SO4 / CH2Cl2 / 24 h / Ambient temperature View Scheme
参考文献
Vankar, Yashwant D.; Chaudhuri, Narayan C.; Rao, C. Trinadha
Tetrahedron Letters, 1987 , vol. 28, # 5 p. 551 - 554
