反应条件
2: 1. BuLi, 2. paraformaldehyde / 1. pentane, ether, -10 deg C, 0.5 h, 2a. THF, 20 deg C, 45 min, 2b. reflux, 2.5 h
3: LiAlH4, CH3OH / diethyl ether; tetrahydrofuran / 2 h / Ambient temperature
View Scheme
参考文献
Khrimyan, A. P.; Makaryan, G. M.; Ovanisyan, A. L.; Wimmer, Z.; Romanyuk, M.; et al.
Chemistry of Natural Compounds, 1991 , vol. 27, # 1 p. 103 - 108
Khimiya Prirodnykh Soedinenii, 1991 , # 1 p. 117 - 123
