N-苄氧羰酰基-L-苏氨酸甲酯合成路线 （共 16 条）
反应条件
triethylamine in dichloromethane T=0 - 20°C; Acylation; 3.5 h;
参考文献
Ferreira, Paula M.T.; Maia, Hernani L.S.; Monteiro, Luis S.; Sacramento, Joana
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 24 p. 3697 - 3703
反应条件
sulfuric acid 36 h; Ambient temperature;
参考文献
Kozikowski; Nieduzak; Konoike; Springer
Journal of the American Chemical Society, 1987 , vol. 109, # 17 p. 5167 - 5175
反应条件
trimethylsilyl trifluoromethanesulfonate in dichloromethane T=0°C; 4 h;
参考文献
Poon, Kevin W. C.; Lovell, Kimberly M.; Dresner, Kendra N.; Datta, Apurba
Journal of Organic Chemistry, 2008 , vol. 73, # 2 p. 752 - 755
反应条件
water; trifluoroacetic acid in dichloromethane T=20°C; Hydrolysis; 14 h;
参考文献
Wipf, Peter; Uto, Yoshikazu
Journal of Organic Chemistry, 2000 , vol. 65, # 4 p. 1037 - 1049
反应条件
in chloroform T=25°C; 1 h;
参考文献
Akhtar; Gani
Tetrahedron, 1987 , vol. 43, # 22 p. 5341 - 5349
反应条件
1: 99 percent / sodium bicarbonate / H2O / 20 °C 2: 97 percent / SOCl2 / 24 h / 20 °C View Scheme
参考文献
Tetrahedron, , vol. 56, # 29 p. 5077 - 5083
反应条件
1.1: CF3COOH / CHCl3; methanol / 0 °C 1.2: 96 percent / NaHCO3 / H2O; ethyl acetate / 20 °C 2.1: 88 percent / BF3*OEt2 / 20 °C 3.1: 69 percent / CF3COOH; H2O / CH2Cl2 / 14 h / 20 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 65, # 4 p. 1037 - 1049
反应条件
1: 88 percent / BF3*OEt2 / 20 °C 2: 69 percent / CF3COOH; H2O / CH2Cl2 / 14 h / 20 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 65, # 4 p. 1037 - 1049
反应条件
dipotassium hydrogenphosphate 1 h; Reflux;
参考文献
Shinada, Tetsuro; Hamada, Makoto; Miyoshi, Kota; Higashino, Masato; Umezawa, Taiki; Ohfune, Yasufumi
Synlett, 2010 , # 14 art. no. U03510ST, p. 2141 - 2145
反应条件
hydrogenchloride T=0°C; 0.5 h; Yield given;
参考文献
Journal of Organic Chemistry, , vol. 62, # 25 p. 8911 - 8913
