1: 2-methoxy-phenol With sodium hydride in N,N-dimethyl-formamide; mineral oil T=20°C; 0.5 h; Inert atmosphereSonication; 2: 1-bromo-3-chloro-1-phenylpropane in N,N-dimethyl-formamide; mineral oil T=20°C; 12 h; Inert atmosphere;

暂无反应条件数据

1.1: N-bromosuccinmide; dibenzoyl peroxide / chlorobenzene / 4 h / 85 °C 2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 20 °C / |Inert atmosphere; |Sonication 2.2: 12 h / 20 °C / |Inert atmosphere View Scheme

methylamine in methanol

tetra-(n-butyl)ammonium iodide; potassium carbonate T=80°C; 24 h; Sealed tube;