1-苯基-1H-[1,2,4]三唑-3-甲酸甲酯合成路线 (共 14 条)
反应条件
in benzene
T=80°C; 4 h;
参考文献
Bruche, Luca; Garanti, Luisa; Zecchi, Gaetano
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 7 p. 1427 - 1429
反应条件
in benzene
T=80°C; 5 h;
参考文献
Bruche, Luca; Garanti, Luisa; Zecchi, Gaetano
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 7 p. 1427 - 1429
反应条件
in benzene
54 h; Heating;
参考文献
Bruche, Luca; Garanti, Luisa; Zecchi, Gaetano
Synthesis, 1985 , # 3 p. 304 - 305
反应条件
in benzene
T=80°C; 3 h;
参考文献
Bruche, Luca; Garanti, Luisa; Zecchi, Gaetano
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 7 p. 1427 - 1429
反应条件
in benzene
T=25°C; 96 h; Further byproducts given;
参考文献
Bruche, Luca; Garanti, Luisa; Zecchi, Gaetano
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1903 - 1906
反应条件
1: 59 percent / sodium azide, hexadecyltributylphosphonium bromide / benzene; H2O / 5 h / 40 °C
2: 8 percent / benzene / 4 h / 80 °C
View Scheme
参考文献
Bruche, Luca; Garanti, Luisa; Zecchi, Gaetano
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 7 p. 1427 - 1429
反应条件
in diethyl ether
6 h; Ambient temperature;
参考文献
Bruche, Luca; Garanti, Luisa; Zecchi, Gaetano
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1903 - 1906
反应条件
in benzene
T=25°C; 96 h; Further byproducts given;
参考文献
Bruche, Luca; Garanti, Luisa; Zecchi, Gaetano
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1903 - 1906
反应条件
1: 85 percent / diethyl ether / 1 h / Heating
2: 53 percent / benzene / 54 h / Heating
View Scheme
参考文献
Bruche, Luca; Garanti, Luisa; Zecchi, Gaetano
Synthesis, 1985 , # 3 p. 304 - 305
反应条件
in 1,4-dioxane
2 h; Heatingbenzene, 4 h; Further byproducts given;
参考文献
Bruche, Luca; Garanti, Luisa; Zecchi, Gaetano
Journal of Heterocyclic Chemistry, 1989 , vol. 26, # 26 p. 619 - 624