2,5-二甲基噻吩-3-羰酰氯合成路线 （共 6 条）
反应条件
palladium on activated charcoal; xylene Hydrogenation;
参考文献
Brown; Blanchette
Journal of the American Chemical Society, 1950 , vol. 72, p. 3414
反应条件
thionyl chloride; N,N-dimethyl-formamide
T=20°C; 3 h;
参考文献
Belen'kii; Gromova; Kolotaev; Nabatov; Krayushkin
Russian Chemical Bulletin, 2005 , vol. 54, # 5 p. 1208 - 1213
反应条件
1: 60 percent / TiCl4 / CH2Cl2 / 2 h / 5 °C
2: 65 percent / CrO3; H2O; H2SO4 / acetone / 6 h / 20 °C
3: 65 percent / thionyl chloride; DMF / 3 h / 20 °C
View Scheme
参考文献
Belen'kii; Gromova; Kolotaev; Nabatov; Krayushkin
Russian Chemical Bulletin, 2005 , vol. 54, # 5 p. 1208 - 1213
反应条件
1: 65 percent / CrO3; H2O; H2SO4 / acetone / 6 h / 20 °C
2: 65 percent / thionyl chloride; DMF / 3 h / 20 °C
View Scheme
参考文献
Belen'kii; Gromova; Kolotaev; Nabatov; Krayushkin
Russian Chemical Bulletin, 2005 , vol. 54, # 5 p. 1208 - 1213
反应条件
1: aqueous sodium hypobromite solution
2: thionyl chloride
View Scheme
参考文献
Buu-Hoi; Nguyen-Hoan
Recueil des Travaux Chimiques des Pays-Bas, 1948 , vol. 67, p. 309,325
反应条件
aluminium trichloride in dichloromethane
参考文献
Belen'kii; Gromova; Kolotaev; Nabatov; Krayushkin
Russian Chemical Bulletin, 2005 , vol. 54, # 5 p. 1208 - 1213
