2,4-二硝基-5-氟苯基叠氮化物合成路线 （共 2 条）
反应条件
1: With sulfuric acid; sodium nitrite in acetic acid
T=0°C;
2: With sodium azide
T=20°C; 1 h;
参考文献
Okiyama, Natsuko; Uchiyama, Seiichi; Onoda, Maki; Imai, Kazuhiro; Santa, Tomofumi
Heterocycles, 2002 , vol. 58, p. 165 - 173
反应条件
1: 810 mg / ethyl acetate / 2.5 h / Heating
2: 52 percent / triphenylphosphine / ethyl acetate / 1 h / Heating
3: 4.7 percent / conc. hydrochloric acid; iron powder / CH2Cl2; methanol / 0.25 h / 20 °C
View Scheme
参考文献
Okiyama, Natsuko; Uchiyama, Seiichi; Onoda, Maki; Imai, Kazuhiro; Santa, Tomofumi
Heterocycles, 2002 , vol. 58, p. 165 - 173
