N-叔丁氧羰基-1,2-乙二胺合成路线 （共 68 条）
反应条件
in chloroform 1.) 3 h, ice bath, 2.) room temperature, 16 h;
参考文献
Jensen, Kim B.; Braxmeier, Tobias M.; Demarcus, Mariangela; Frey, Jeremy G.; Kilburn, Jeremy D.
Chemistry - A European Journal, 2002 , vol. 8, # 6 p. 1300 - 1309
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Wang, Jun; Uttamchandani, Mahesh; Li, Junqi; Hu, Mingyu; Yao, Shao Q.
Chemical Communications, 2006 , # 36 p. 3783 - 3785
反应条件
ethylenediamine in 1,4-dioxane; dichloromethane; water
参考文献
Merrell Pharmaceuticals Inc.
Patent: US5604221 A1, 1997 ;
反应条件
ammonia; hydrogen; nickel in ethanol P=2585.7 Torr; 14 h; Ambient temperature;
参考文献
Ravikumar
Synthetic Communications, 1994 , vol. 24, # 12 p. 1767 - 1772
反应条件
in chloroform 2 h; Ambient temperature;
参考文献
Demonchaux; Granellin; Dunn; Haylett; Jenkinson
European Journal of Medicinal Chemistry, 1991 , vol. 26, # 9 p. 915 - 920
反应条件
in tetrahydrofuran T=45°C; Condensation; 0.333333 h;
参考文献
Karki, Laba; Lakshmi; Szalai, Veronika A.; Brudvig, Gary W.
Journal of the American Chemical Society, 2000 , vol. 122, # 21 p. 5180 - 5188
参考文献
Pittelkow, Michael; Lewinsky, Rasmus; Christensen, Jorn Bolstad
Synthesis, 2002 , # 15 p. 2195 - 2202
反应条件
in 1,4-dioxane; water
参考文献
Caldarelli, Francesco; Ceriani, Lucio; Candiani, Ilaria
Patent: US2004/77550 A1, 2004 ;
反应条件
dimethylsulfide borane complex in tetrahydrofuran; dichloromethane T=20°C; 24.3333 h; RefluxInert atmosphere;
参考文献
Xu, Zhigang; DiCesare, John C.; Baures, Paul W.
Journal of Combinatorial Chemistry, 2010 , vol. 12, # 2 p. 248 - 254
反应条件
hydrazine hydrate in ethanol
反应条件
5 Pd(II)/C(eggshell); hydrogen in methanol 18 h;
参考文献
Xu, Zhigang; DiCesare, John C.; Baures, Paul W.
Journal of Combinatorial Chemistry, 2010 , vol. 12, # 2 p. 248 - 254
