3-羟基-7,12-二甲基苯并(a)蒽合成路线 （共 13 条）
反应条件
1: 88 percent / Adogen 464, Fremy's salt, KH2PO4 / H2O; benzene / 0.5 h
2: 79 percent / NaBH4 / ethanol
3: m-CPBA / CH2Cl2 / 1 h / Ambient temperature
View Scheme
参考文献
Lee; Harvey
Journal of Organic Chemistry, 1986 , vol. 51, # 18 p. 3502 - 3507
反应条件
1: 0.10 g / o-iodoxybenzoic acid / dimethylformamide / 0.17 h
2: NaBH4; O2
View Scheme
参考文献
Lee; Harvey
Journal of Organic Chemistry, 1986 , vol. 51, # 18 p. 3502 - 3507
反应条件
1: 83 percent / Fermy's salt, KH2PO4, H2O / benzene / 0.5 h
2: 94 percent / NaBH4, O2 / ethanol / 72 h
3: N-bromosuccinimide / dimethylsulfoxide; H2O / 30 h
View Scheme
参考文献
Lee; Harvey
Journal of Organic Chemistry, 1986 , vol. 51, # 18 p. 3502 - 3507
