bis-triphenylphosphine-palladium(II) chloride; triethylamine in benzene
T=100°C; P=30400 Torr; 24 h; Title compound not separated from byproducts;
参考文献
Negishi, Ei-Ichi; Coperet, Christophe; Ma, Shengming; Mita, Takeshi; Sugihara, Takumichi; Tour, James M.
Journal of the American Chemical Society, 1996 , vol. 118, # 25 p. 5904 - 5918
Negishi, Ei-Ichi; Coperet, Christophe; Ma, Shengming; Mita, Takeshi; Sugihara, Takumichi; Tour, James M.
Journal of the American Chemical Society, 1996 , vol. 118, # 25 p. 5904 - 5918
1: With benzotriazol-1-ol; dacarbazine in N,N-dimethyl-formamide
Condensation;
2: With hexafluoroisopropyl alcohol; dihydrogen peroxide in dichloromethane
Oxidation; Solid phase reaction;
3: in 1,4-dioxane
T=100°C; Elimination;
参考文献
Russell, Helen E.; Luke, Richard W.A.; Bradley, Mark
Tetrahedron Letters, 2000 , vol. 41, # 27 p. 5287 - 5290