N-(4-甲氧基苄基)苯-1,2-二胺合成路线 （共 9 条）
反应条件
ammonia; hydrogen; nickel in methanol
P=37510.9 Torr;
参考文献
Zellner,H.; Zellner,G.
Helvetica Chimica Acta, 1966 , vol. 49, p. 913 - 939
反应条件
2: H2, NH3 / Raney-Ni / methanol / 37510.9 Torr
View Scheme
参考文献
Zellner,H.; Zellner,G.
Helvetica Chimica Acta, 1966 , vol. 49, p. 913 - 939
反应条件
2: H2, NH3 / Raney-Ni / methanol / 37510.9 Torr
View Scheme
参考文献
Zellner,H.; Zellner,G.
Helvetica Chimica Acta, 1966 , vol. 49, p. 913 - 939
反应条件
triethylamine in tetrahydrofuran
21 h; Reflux;
参考文献
Vlaar, Tjostil; Cioc, Razvan C.; Mampuys, Pieter; Maes, Bert U. W.; Orru, Romano V. A.; Ruijter, Eelco
Angewandte Chemie - International Edition, 2012 , vol. 51, # 52 p. 13058 - 13061
Angew. Chem., 2012 , vol. 124, # 52 p. 13235 - 13238,4
反应条件
nickel; ethyl acetate
T=50°C; P=110326 Torr; Hydrogenation;
参考文献
Schering A.G.
Patent: DE901649 , 1951 ;
反应条件
potassium carbonate in N,N-dimethyl-formamide
T=20°C; 4 h;
参考文献
Xue, Ding; Long, Ya-Qiu
Journal of Organic Chemistry, 2014 , vol. 79, # 10 p. 4727 - 4734
反应条件
1: methanol
2: Raney nickel; ethyl acetate / 50 °C / 110326 Torr / Hydrogenation
View Scheme
参考文献
Schering A.G.
Patent: DE901649 , 1951 ;
反应条件
1: methanol
2: Raney nickel; ethyl acetate / 50 °C / 110326 Torr / Hydrogenation
View Scheme
参考文献
Schering A.G.
Patent: DE901649 , 1951 ;
反应条件
2,2,6,6-tetramethyl-1-piperidinyloxy, free radical in N,N-dimethyl-formamide
T=110°C; 5 h;
参考文献
Xue, Ding; Long, Ya-Qiu
Journal of Organic Chemistry, 2014 , vol. 79, # 10 p. 4727 - 4734
