反应条件
1.1: thionyl chloride; triethylamine / dichloromethane / 1 h / 20 °C 2.1: sodium periodate; ruthenium trichloride / dichloromethane; water; acetonitrile / 2 h / 20 °C 3.1: tetra-(n-butyl)ammonium iodide; 1,8-diazabicyclo[5.4.0]undec-7-ene / toluene / 5 h / 70 °C / Reflux 3.2: 3 h / 22 °C 4.1: hydrogenchloride / tetrahydrofuran; water / 3 h 4.2: 1 h / Reflux View Scheme
参考文献
Van Den Berg, Richard J. B. H. N.; Van Den Elst, Hans; Korevaar, Cornelius G. N.; Aerts, Johannes M. F. G.; Van Der Marel, Gijsbert A.; Overkleeft, Herman S.
European Journal of Organic Chemistry, 2011 , # 33 p. 6685 - 6689