1-(3-溴丙基)-4-甲氧基苯合成路线 （共 22 条）
反应条件
lithium bromide in acetone
24 h; Yield given;
参考文献
Mohamed, Salah E.N.; Whiting, Donald A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 10 p. 2577 - 2582
反应条件
1: (i) Mg, (ii) /BRN= 605308/
2: HBr, (PhCO)2O2 / toluene
View Scheme
参考文献
Delobelle,J.; Fetizon,M.
Bulletin de la Societe Chimique de France, 1961 , p. 1894 - 1900
反应条件
1: sodium
2: tetrachloromethane; PBr3 / 60 °C
View Scheme
参考文献
Horeau
Bulletin de la Societe Chimique de France, 1948 , p. 414,416
反应条件
1: sodium
2: tetrachloromethane; PBr3 / 60 °C
View Scheme
参考文献
Horeau
Bulletin de la Societe Chimique de France, 1948 , p. 414,416
参考文献
Kin<Kim>
Yakugaku Zasshi, 1943 , vol. 63, p. 376,381
Chem.Abstr., 1951 , p. 5126
反应条件
1: ethanol / Erwaermen des Reaktionsprodukts mit wss. Kalilauge
2: 130 °C
View Scheme
参考文献
van der Zanden
Recueil des Travaux Chimiques des Pays-Bas, 1938 , vol. 57, p. 233,243
反应条件
1: 1.) thiourea, 2.) 10percent NaOH / 1.) EtOH, reflux, 4 h, 2.) H2O, 80 deg C, 2 h
2: 71 percent / Na, EtOH / 1.5 h / Heating
View Scheme
参考文献
Mohamed, Salah E.N.; Whiting, Donald A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 10 p. 2577 - 2582
反应条件
1: 1.) thiourea, 2.) 10percent NaOH / 1.) EtOH, reflux, 4 h, 2.) H2O, 80 deg C, 2 h
2: 71 percent / Na, EtOH / 1.5 h / Heating
3: 58 percent / m-chloroperbenzoic acid / CH2Cl2 / 6 h
View Scheme
参考文献
Mohamed, Salah E.N.; Whiting, Donald A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 10 p. 2577 - 2582
反应条件
1: Mg / diethyl ether / Heating
2: CrO3, aq. AcOH
View Scheme
参考文献
Delobelle,J.; Fetizon,M.
Bulletin de la Societe Chimique de France, 1961 , p. 1894 - 1900
反应条件
diethyl ether; sodium
参考文献
Delobelle,J.; Fetizon,M.
Bulletin de la Societe Chimique de France, 1961 , p. 1894 - 1900
