反应条件
1.1: n-ethyl morpholine; copper(l) chloride; copper / 16 h / 70 °C / |Inert atmosphere
2.1: sodium tetrahydroborate; sodium ethanolate / ethanol / 24 h / 65 °C / |Inert atmosphere
3.1: triethylamine; diphenyl phosphoryl azide / tetrahydrofuran / 3 h / 20 °C / |Inert atmosphere
3.2: 2 h / |Inert atmosphere; |Reflux
View Scheme
参考文献
Borrero, Nicholas V.; Bai, Fang; Perez, Cristian; Duong, Benjamin Q.; Rocca, James R.; Jin, Shouguang; Huigens Iii, Robert W.
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 6 p. 881 - 886