4’-硝基[1,1’-联苯]-4-甲酸甲酯合成路线 (共 19 条)
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium carbonate in water; N,N-dimethyl-formamide T=55°C; 19 h;
参考文献
Adachi, Yusuke; Nakagawa, Hidehiko; Matsuo, Kazuya; Suzuki, Takayoshi; Miyata, Naoki
Chemical Communications, 2008 , # 41 p. 5149 - 5151
反应条件
thionyl chloride T=70°C;
参考文献
Venkatraj, Muthusamy; Messagie, Jonas; Joossens, Jurgen; Lambeir, Anne-Marie; Haemers, Achiel; Van Der Veken, Pieter; Augustyns, Koen
Bioorganic and Medicinal Chemistry, 2012 , vol. 20, # 4 p. 1557 - 1568
反应条件
palladium on activated charcoal in m-xylene T=140°C; 10 h;
参考文献
Matsushita; Sakamoto; Murakami; Matsui
Synthetic Communications, 1994 , vol. 24, # 22 p. 3307 - 3313
反应条件
potassium carbonate in N,N-dimethyl-formamide T=110°C; Suzuki Coupling; 4 h; Inert atmosphere;
参考文献
Arundhathi, Racha; Damodara, Dandu; Mohan, Kakita Veera; Kantam, Mannepalli Lakshmi; Likhar, Pravin R.
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 4 p. 751 - 756
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene T=110°C; Stille Cross Coupling; 12 h; Inert atmosphere;
参考文献
Qiu, Di; Meng, He; Jin, Liang; Wang, Shuai; Tang, Shengbo; Wang, Xi; Mo, Fanyang; Zhang, Yan; Wang, Jianbo
Angewandte Chemie - International Edition, 2013 , vol. 52, # 44 p. 11581 - 11584
Angew. Chem., 2013 , vol. 125, # 44 p. 11795 - 11798
反应条件
nitric acid in acetic anhydride
参考文献
Journal of Organometallic Chemistry, , vol. 117, p. 35 - 54
反应条件
1: aq. NaOBr / dioxane 2: (i) SOCl2, (ii) /BRN= 1098229/ View Scheme
参考文献
Journal of the Chemical Society [Section] C: Organic, , p. 840 - 845
反应条件
1: AlCl3 / nitrobenzene 2: aq. NaOBr / dioxane 3: (i) SOCl2, (ii) /BRN= 1098229/ View Scheme
参考文献
Journal of the Chemical Society [Section] C: Organic, , p. 840 - 845
反应条件
1.1: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / ethanol; water; toluene / 48 h / Inert atmosphere; Reflux 1.2: pH 3 2.1: thionyl chloride / 70 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 20, # 4 p. 1557 - 1568
反应条件
1.1: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / ethanol; water; toluene / 48 h / Inert atmosphere; Reflux 1.2: pH 3 2.1: thionyl chloride / 70 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 20, # 4 p. 1557 - 1568