4-乙酰基-4-溴代联苯合成路线 （共 24 条）
反应条件
AlCl3, aluminium chloride in dichloromethane T=15°C; 10.5 h; Cooling with ice;
参考文献
Journal of Molecular Liquids, , vol. 175, p. 72 - 84
反应条件
aluminium trichloride in carbon disulfide 1 h; Heating;
参考文献
Journal of the American Chemical Society, , vol. 107, # 21 p. 6046 - 6052
反应条件
tetrakis(triphenylphosphine) palladium(0); caesium carbonate in N,N-dimethyl-formamide T=80°C; 18 h;
参考文献
Journal of Organic Chemistry, , vol. 68, # 9 p. 3729 - 3732
反应条件
1: 4,4'-dibromo biphenyl With (nBu)3MgLi in tetrahydrofuran; hexane T=0°C; 1.5 h; 2: acetic anhydride in tetrahydrofuran; hexane T=-20°C; 1 h;
参考文献
Tetrahedron, , vol. 62, # 21 p. 5092 - 5098
反应条件
palladium 10 on activated carbon in methanol Suzuki-Miyaura cross-coupling; RefluxUnder air;
参考文献
Letters in Organic Chemistry, , vol. 7, # 1 p. 1 - 6
反应条件
1: palladium(II) acetate; potassium acetate / dimethylformamide / 18 h / 80 °C 2: 75 percent / Cs2CO3; Pd(PPh3)4 / dimethylformamide / 18 h / 80 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 68, # 9 p. 3729 - 3732
反应条件
according to ref. 9.;
参考文献
Tetrahedron Letters, , vol. 25, # 43 p. 4909 - 4912
反应条件
in 1,4-dioxane; water T=30°C; Equilibrium constant;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 749 - 750
反应条件
pyridine; palladium diacetate; potassium carbonate T=120°C; 6 h; Ionic liquid;
参考文献
Xin, Bingwei; Jia, Chunxiao; Qi, Zhixun
Journal of Chemical Research, 2012 , vol. 36, # 7 p. 407 - 410
反应条件
1: aq. NaOBr / dioxane 2: Py / dimethylformamide View Scheme
参考文献
Byron,D.J. et al.
Journal of the Chemical Society [Section] C: Organic, 1966 , p. 840 - 845
