(1-甲基萘-4-基)甲醇合成路线 （共 20 条）
反应条件
Catalyst M-Chromium oxide; sulfuric acid T=60 - 65°C;
参考文献
Ziegler; Tiemann
Chemische Berichte, 1922 , vol. 55, p. 3414
反应条件
potassium permanganate
参考文献
Lock; Schneider
Chemische Berichte, 1951 , vol. 84, p. 636,640
反应条件
borane in tetrahydrofuran
1 h; Ambient temperature;
参考文献
DeCosta, Dayal P.; Pincock, James A.
Journal of the American Chemical Society, 1993 , vol. 115, # 6 p. 2180 - 2190
反应条件
amberlyst-15; 4 A molecular sieve in tetrahydrofuran
T=25°C; 3 h;
参考文献
Jefford, Charles W.; Rossier, Jean-Claud; Kohmoto, Shigeo; Boukouvalas, John
Helvetica Chimica Acta, 1985 , vol. 68, p. 1804 - 1814
反应条件
sulfuric acid in tetrahydrofuran
T=25°C; 3 h;
参考文献
Jefford, Charles W.; Rossier, Jean-Claude; Kohmoto, Shigeo; Boukouvalas, John
Journal of the Chemical Society, Chemical Communications, 1984 , # 22 p. 1496 - 1497
反应条件
1: dimethylformamide / 6 h / Heating
2: 2.5 M NaOH / ethanol / 24 h / Heating
3: 90 percent / BH3 / tetrahydrofuran / 1 h / Ambient temperature
View Scheme
参考文献
DeCosta, Dayal P.; Pincock, James A.
Journal of the American Chemical Society, 1993 , vol. 115, # 6 p. 2180 - 2190
反应条件
1: 2.5 M NaOH / ethanol / 24 h / Heating
2: 90 percent / BH3 / tetrahydrofuran / 1 h / Ambient temperature
View Scheme
参考文献
DeCosta, Dayal P.; Pincock, James A.
Journal of the American Chemical Society, 1993 , vol. 115, # 6 p. 2180 - 2190
反应条件
sulfuric acid in tetrahydrofuran
T=25°C; 3 h; Further byproducts given;
参考文献
Jefford, Charles W.; Rossier, Jean-Claud; Kohmoto, Shigeo; Boukouvalas, John
Helvetica Chimica Acta, 1985 , vol. 68, p. 1804 - 1814
反应条件
sulfuric acid in tetrahydrofuran
T=25°C; 3 h; Further byproducts given;
参考文献
Jefford, Charles W.; Rossier, Jean-Claud; Kohmoto, Shigeo; Boukouvalas, John
Helvetica Chimica Acta, 1985 , vol. 68, p. 1804 - 1814
反应条件
amberlyst-15; dihydrogen peroxide in diethyl ether
T=25°C; 4 h;
参考文献
Jefford, Charles W.; Rossier, Jean-Claud; Kohmoto, Shigeo; Boukouvalas, John
Helvetica Chimica Acta, 1985 , vol. 68, p. 1804 - 1814
