2-十一烷基-1,3-二氧戊环合成路线 （共 8 条）
反应条件
1.1: 56 percent / acetophenone / 14 h / Irradiation 2.1: NaHMDS / tetrahydrofuran / -98 °C 2.2: 36 percent / -98 °C 3.1: 97 percent / montmorillonite K10 / CH2Cl2 / Heating 4.1: H2 / Rh/alumina / ethyl acetate / 5320 - 6080 Torr 5.1: DEAD; PPh3 / tetrahydrofuran / 0 - 25 °C View Scheme
参考文献
Parsons, Philip J.; Cowell, Justin K.
Synlett, 2000 , # 1 p. 107 - 109
反应条件
CoCl2.6H2O; zinc in tetrahydrofuran T=20°C; 4 h;
参考文献
Sarma, Kuladip; Goswami, Amrit
Letters in Organic Chemistry, 2009 , vol. 6, # 7 p. 568 - 572
反应条件
1,3-bis(2,6-diisopropylphenyl)imidazolinium chloride; tris(dibenzylideneacetone)dipalladium (0) in tetrahydrofuran; 1-methyl-pyrrolidin-2-one
T=20°C; Negishi cross-coupling; 24 h;
参考文献
Hadei, Niloufar; Kantchev, Eric Assen B.; O'Brien, Christopher J.; Organ, Michael G.
Journal of Organic Chemistry, 2005 , vol. 70, # 21 p. 8503 - 8507
反应条件
dimethyl sulfoxide; [ReV(O)Cl3(PPh3)2] in toluene
23 h; Heating;
参考文献
Arterburn, Jeffrey B.; Perry, Marc C.
Organic Letters, 1999 , vol. 1, # 5 p. 769 - 771
反应条件
camphor-10-sulfonic acid in dichloromethane
T=20°C;
参考文献
Maegawa, Tomohiro; Otake, Kazuki; Goto, Akihiro; Fujioka, Hiromichi
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 16 p. 5648 - 5651
反应条件
in ethylene glycol; toluene
参考文献
Macro Chem. Corp.
Patent: US4861764 A1, 1989 ;
反应条件
iodine; mercury(II) oxide in benzene
4.5 h; Irradiation;
参考文献
Suginome, Hiroshi; Wang, Jian Bo
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 10 p. 2825 - 2829
反应条件
nitrogen(IV) oxide; silica gel
参考文献
Nishiguchi, Takeshi; Ohosima, Tatsuya; Nishida, Akiko; Fujisaki, Shizuo
Journal of the Chemical Society, Chemical Communications, 1995 , # 11 p. 1121 - 1122
