2,2-二甲基-1,3-二氧戊环-4-甲醛合成路线 （共 10 条）
反应条件
2,6-dimethylpyridine; oxoammonium salt in dichloromethane 4 h; Inert atmosphere;
参考文献
Bobbitt, James M.; Bartelson, Ashley L.; Bailey, William F.; Hamlin, Trevor A.; Kelly, Christopher B.
Journal of Organic Chemistry, 2014 , vol. 79, # 3 p. 1055 - 1067
反应条件
lead(IV) acetate in benzene
参考文献
Heathcock, Clayton H.; Pirrung, Michael C.; Lampe, John; Buse, Charles T.; Young, Steven D.
Journal of Organic Chemistry, 1981 , vol. 46, # 11 p. 2290 - 2300
反应条件
toluene-4-sulfonic acid in N,N-dimethyl-formamide T=20°C; 20 h;
参考文献
Chemical Communications, , # 1 p. 124 - 126
反应条件
pyridinium chlorochromate
参考文献
WO2007/124136 A1, ;
Page/Page column 170 ;
WO 2007/124136 A1
反应条件
sodium periodate in ethanol; water T=0°C;
参考文献
Liebigs Annalen der Chemie, , # 3 p. 412 - 424
反应条件
sodium periodate; silica gel in dichloromethane 0.25 h;
参考文献
Daumas, M.; Vo-Quang, Y.; Vo-Quang, L.; Goffic, F. Le
Synthesis, 1989 , # 1 p. 64 - 65
反应条件
acetone; zinc(II) chloride
参考文献
Chemische Berichte, , vol. 63, p. 1749,1751
Helvetica Chimica Acta, , vol. 17, p. 622,631
Helvetica Chimica Acta, , vol. 17, p. 627
Helvetica Chimica Acta, , vol. 19, p. 524
参考文献
Chemische Berichte, , vol. 63, p. 1749,1751
Helvetica Chimica Acta, , vol. 17, p. 622,631
反应条件
sodium tetrahydroborate in ethanol 1 h; Ambient temperature;
参考文献
Huss, Keith E. Maloney
Synthetic Communications, 1985 , vol. 15, # 4 p. 273 - 278
反应条件
1: With polymethylhydrosiloxane; ferrous acetate; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=65°C; 16 h; 2: With sodium hydrogencarbonate in tetrahydrofuran; methanol T=0 - 20°C; Further stages.;
参考文献
Shaikh, Nadim S.; Junge, Kathrin; Beller, Matthias
Organic Letters, 2007 , vol. 9, # 26 p. 5429 - 5432
