1-(4-氯苯基)-3-苯基-1-丙酮合成路线 (共 28 条)
反应条件
benzaldehyde; potassium hydroxide T=110°C; 32 h; Schlenk techniqueInert atmosphereGreen chemistry;
参考文献
Xu, Qing; Chen, Jianhui; Liu, Quan
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 4 p. 697 - 704
参考文献
Bunce, Nigel J.; Bergsma, John P.; Bergsma, Michael D.; Graaf, Wilma de; Kumar, Yogesh; Ravanal, Luis
Journal of Organic Chemistry, 1980 , vol. 45, # 18 p. 3708 - 3713
反应条件
2,2'-azo-bisisobutyronitrile T=75°C;
参考文献
Journal of Organic Chemistry, , vol. 35, p. 3192 - 3195
反应条件
trifluoroacetic acid 72 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 72, # 24 p. 9383 - 9386
反应条件
1: sodium hydroxide / ethanol / 4 h / 0 - 20 °C 2: acetoxy(2,6-bis((diphenylphosphino)methyl)-3,5-dimethylphenyl)palladium(II); butan-1-ol; potassium carbonate / 1 h / |Reflux View Scheme
参考文献
Organic Letters, , vol. 15, # 14 p. 3690 - 3693
反应条件
sodium formate in water T=100°C; 12 h; chemoselective reaction;
参考文献
Green Chemistry, , vol. 13, # 6 p. 1490 - 1494
反应条件
1: 90 percent / sodium borohydride; nickel(II) chloride hexahydrate / methanol; H2O / 0.5 h / 20 °C View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 77, # 3 p. 549 - 552
反应条件
Rhizopus arrhizus NCIM 878 in ethanol; water T=30°C; pH=4.5 - 4.8; Microbiological reaction;
参考文献
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, , vol. 49, # 2 p. 199 - 202
反应条件
potassium phosphate; Wilkinson's catalyst; 2,2'-bis-(diphenylphosphino)-1,1'- binaphthyl in 1,4-dioxane T=80°C; 20 h; Inert atmosphere; Overall yield = 57 percent; Overall yield = 136 mg;
参考文献
Advanced Synthesis and Catalysis, , vol. 355, # 9 p. 1874 - 1880
反应条件
1: 90 percent / sodium borohydride; nickel(II) chloride hexahydrate / methanol; H2O / 0.5 h / 20 °C View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 77, # 3 p. 549 - 552