1-(4-甲氧基苯基)-3-苯基-丙-1-酮合成路线 （共 53 条）
反应条件
triethylamine; triphenylphosphine; palladium diacetate T=100°C; Arylation; Heck; 7 h;
参考文献
Synthetic Communications, , vol. 28, # 12 p. 2311 - 2316
反应条件
1: palladium on activated charcoal; hydrogen / ethanol / 20 °C / 760.05 Torr 2: 1-methoxy-4-chlorobenzene; caesium carbonate; palladium diacetate; dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine / water; tert-butyl alcohol / 16 h / 95 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 134, # 40 p. 16856 - 16868,13
Journal of the American Chemical Society, , vol. 134, # 40 p. 16856 - 16868
反应条件
SiClO4; p-trifluoromethylthiobenzoic anhydride; silver perchlorate in dichloromethane 63 h; Ambient temperature;
参考文献
Suzuki; Kitagawa; Mukaiyama
Bulletin of the Chemical Society of Japan, 1993 , vol. 66, # 12 p. 3729 - 3734
反应条件
tris(triphenylphosphine)ruthenium(II) chloride; dodec-1-ene; potassium hydroxide in 1,4-dioxane T=80°C; 40 h;
参考文献
Cho, Chan Sik; Kim, Bok Tae; Yoon, Nam Sik
Applied Organometallic Chemistry, 2011 , vol. 25, # 9 p. 695 - 698
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene Heating;
参考文献
Boger, Dale L.; Mathvink, Robert J.
Journal of Organic Chemistry, 1989 , vol. 54, # 8 p. 1777 - 1779
反应条件
1: 85 percent / sodium borohydride; nickel(II) chloride hexahydrate / methanol; H2O / 0.5 h / 20 °C View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 77, # 3 p. 549 - 552
反应条件
1: 2-phenoxy-1-(4-methoxyphenyl)-ethanol With tris(triphenylphosphine)ruthenium(II) chloride; potassium 2-methyl-2-butoxide; ethyl acetate in toluene T=140°C; 8 h; Schlenk techniqueSealed tubeInert atmosphere; 2: benzyl alcohol With potassium hydroxide in toluene T=140°C; 16 h; Schlenk techniqueSealed tubeInert atmosphere;
参考文献
Weickmann, Daniel; Plietker, Bernd
ChemCatChem, 2013 , vol. 5, # 8 p. 2170 - 2173
反应条件
hydrogen; bis-(ethyl)-phenyl-phosphine; [Ir2(OMe)2(1,5-cyclooctadiene)2] in toluene T=100°C; P=15200 Torr; 24 h; regioselectivity; other phenyl substituted enones; Product distribution;
参考文献
Tetrahedron, , vol. 47, # 10-11 p. 1965 - 1976
反应条件
1: COgen With tri-tert-butyl phosphine; N-ethyl-N,N-diisopropylamine; bis(dibenzylideneacetone)-palladium(0) in 1,4-dioxane Inert atmosphere; 2: styrene; para-iodoanisole With N,N-dicyclohexylmethylamine; palladium diacetate in 1,4-dioxane T=95°C; Heck reaction; 20 h; Inert atmosphere;
参考文献
Organic Letters, , vol. 13, # 9 p. 2444 - 2447
反应条件
1: N,N-dicyclohexylmethylamine; bis(dibenzylideneacetone)-palladium(0); cataCXium PIntB / N,N-dimethyl-formamide / 1 h / 100 °C / Inert atmosphere 2: pyrrolidine / N,N-dimethyl-formamide / 6 h / 115 °C / Inert atmosphere View Scheme
参考文献
Organic Letters, , vol. 13, # 20 p. 5456 - 5459
